O-Phenylacetyl-N-<1-oxo-1-phenyl-propyliden-(2)>-hydroxylamin

Base Information

• Chemical Name: O-Phenylacetyl-N-<1-oxo-1-phenyl-propyliden-(2)>-hydroxylamin
• CAS No.: 19347-16-1
• Molecular Formula: C₁₇H₁₅NO₃
• Molecular Weight: 281.311
• Mol file: 19347-16-1.mol

Synonyms:O-Phenylacetyl-N-<1-oxo-1-phenyl-propyliden-(2)>-hydroxylamin

Chemical Property of O-Phenylacetyl-N-<1-oxo-1-phenyl-propyliden-(2)>-hydroxylamin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of O-Phenylacetyl-N-<1-oxo-1-phenyl-propyliden-(2)>-hydroxylamin

There total 2 articles about O-Phenylacetyl-N-<1-oxo-1-phenyl-propyliden-(2)>-hydroxylamin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-phenyl-1,2-propanedione 2-oxime (119-51-7) + phenylacetyl chloride (103-80-0) → O-Phenylacetyl-N-<1-oxo-1-phenyl-propyliden-(2)>-hydroxylamin (19347-16-1)

Guidance literature:

With triethylamine; In dichloromethane; at 38 ℃; for 12h;

DOI:10.1021/acs.orglett.9b03409

Reference yield:

→ O-Phenylacetyl-N-<1-oxo-1-phenyl-propyliden-(2)>-hydroxylamin (19347-16-1)

Guidance literature:

2-Oximino-1-phenyl-propanon-(1), Dicyclohexylcarbodiimid in abs. THF (unter 5grad);

Reference yield: 55.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + O-Phenylacetyl-N-<1-oxo-1-phenyl-propyliden-(2)>-hydroxylamin (19347-16-1) → N-acetyl-N-(3-oxo-1,3-diphenylpropyl)-2-phenylacetamide

Guidance literature:

With mer-tris((2-pyridinyl-κN)phenyl-κ2C)iridium(III); In acetonitrile; at 20 ℃; for 24h; Inert atmosphere; Sealed tube; Irradiation;

DOI:10.1021/acs.orglett.9b03409

upstream raw materials:

1-phenyl-1,2-propanedione 2-oxime

phenylacetyl chloride