ethyl cinnamyl (hydroxymethyl)phosphinate

Base Information

Chemical Name:ethyl cinnamyl (hydroxymethyl)phosphinate
CAS No.:1382936-88-0
Molecular Formula:C₁₂H₁₇O₃P
Molecular Weight:240.239
Hs Code.:

Synonyms:ethyl cinnamyl (hydroxymethyl)phosphinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl cinnamyl (hydroxymethyl)phosphinate

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Technology Process of ethyl cinnamyl (hydroxymethyl)phosphinate

There total 1 articles about ethyl cinnamyl (hydroxymethyl)phosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1207192-25-3
cinnamyl-phosphinic acid ethyl ester

: 1382936-88-0
ethyl cinnamyl (hydroxymethyl)phosphinate

Guidance literature:: With pyridine; In toluene; for 24h; Reflux; Inert atmosphere;
DOI:10.1021/ol3013793

Reference yield:

: 1382936-88-0
ethyl cinnamyl (hydroxymethyl)phosphinate

: 1207192-25-3
cinnamyl-phosphinic acid ethyl ester

Guidance literature:: ethyl cinnamyl (hydroxymethyl)phosphinate; With N-chloro-succinimide; dimethylsulfide; In dichloromethane; at -78 ℃; for 1.33333h; Inert atmosphere;

With triethylamine; In dichloromethane; at -78 - 20 ℃; for 1.25h; Inert atmosphere;
DOI:10.1021/ol3013793