C₁₉H₂₂O₃

Base Information

Chemical Name:C₁₉H₂₂O₃
CAS No.:1478662-54-2
Molecular Formula:C₁₉H₂₂O₃
Molecular Weight:298.382
Hs Code.:

C<sub>19</sub>H<sub>22</sub>O<sub>3</sub>

Synonyms:C₁₉H₂₂O₃

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Chemical Property of C₁₉H₂₂O₃

Chemical Property:

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Technology Process of C₁₉H₂₂O₃

There total 13 articles about C₁₉H₂₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1478662-27-9
C₁₇H₁₆O₂

: 149-73-5
trimethyl orthoformate

: 1478662-54-2
C₁₉H₂₂O₃

Guidance literature:: With Amberlyst-15; In acetonitrile; at 0 - 20 ℃; for 1h;
DOI:10.1055/s-0033-1339484

Reference yield:

: 1477494-06-6
ethyl 7-(4-ethoxycarbonylphenyl)-5-hydroxy-3-methylindan-4-carboxylate

: 1478662-54-2
C₁₉H₂₂O₃

Guidance literature:: Multi-step reaction with 13 steps

1: dimethylsulfide borane complex / tetrahydrofuran / 17 h / 0 - 20 °C

2: triethylamine / dichloromethane / 1.5 h / 0 - 20 °C

3: triethylamine / dichloromethane / 4 h / 0 - 20 °C

4: triphenylphosphine; triethylamine; formic acid; palladium diacetate / N,N-dimethyl-formamide / 2 h / 60 °C

5: lithium borohydride / tetrahydrofuran / 20 h / 0 - 50 °C / Inert atmosphere

6: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 3 h / 0 - 20 °C

7: tetrahydrofuran / 1 h / 0 - 20 °C

8: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 0.5 h / 0 - 20 °C

9: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / 0 - 20 °C

10: 3-chloro-benzenecarboperoxoic acid; scandium tris(trifluoromethanesulfonate) / dichloromethane / 72 h / 0 - 20 °C / Inert atmosphere

11: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 2.5 h / 0 - 20 °C

12: hydrogenchloride / tetrahydrofuran; water / 24 h / 0 - 20 °C

13: Amberlyst-15 / acetonitrile / 1 h / 0 - 20 °C

With hydrogenchloride; lithium borohydride; formic acid; dimethylsulfide borane complex; tetrabutyl ammonium fluoride; palladium diacetate; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; 10: |Baeyer-Villiger Ketone Oxidation;
DOI:10.1055/s-0033-1339484

Reference yield:

: 1477494-13-5
ethyl 4-[7-(tert-butyldimethylsilanyloxymethyl)-1-methylindan-4-yl]benzoate

: 1478662-54-2
C₁₉H₂₂O₃

Guidance literature:: Multi-step reaction with 9 steps

1: lithium borohydride / tetrahydrofuran / 20 h / 0 - 50 °C / Inert atmosphere

2: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 3 h / 0 - 20 °C

3: tetrahydrofuran / 1 h / 0 - 20 °C

4: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 0.5 h / 0 - 20 °C

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / 0 - 20 °C

6: 3-chloro-benzenecarboperoxoic acid; scandium tris(trifluoromethanesulfonate) / dichloromethane / 72 h / 0 - 20 °C / Inert atmosphere

7: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 2.5 h / 0 - 20 °C

8: hydrogenchloride / tetrahydrofuran; water / 24 h / 0 - 20 °C

9: Amberlyst-15 / acetonitrile / 1 h / 0 - 20 °C

With hydrogenchloride; lithium borohydride; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; Dess-Martin periodane; 3-chloro-benzenecarboperoxoic acid; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; dichloromethane; water; acetonitrile; 6: |Baeyer-Villiger Ketone Oxidation;
DOI:10.1055/s-0033-1339484