[(N,N'-bis(2,6-dimethylphenyl)-2,4-pentanediiminato)-bis(trimethylsillylmethylene)chromium(III)]

Base Information

Chemical Name:[(N,N'-bis(2,6-dimethylphenyl)-2,4-pentanediiminato)-bis(trimethylsillylmethylene)chromium(III)]
CAS No.:635683-83-9
Molecular Formula:C₂₉H₄₇CrN₂Si₂
Molecular Weight:531.873
Hs Code.:

Synonyms:[(N,N'-bis(2,6-dimethylphenyl)-2,4-pentanediiminato)-bis(trimethylsillylmethylene)chromium(III)]

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Chemical Property of [(N,N'-bis(2,6-dimethylphenyl)-2,4-pentanediiminato)-bis(trimethylsillylmethylene)chromium(III)]

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Technology Process of [(N,N'-bis(2,6-dimethylphenyl)-2,4-pentanediiminato)-bis(trimethylsillylmethylene)chromium(III)]

There total 1 articles about [(N,N'-bis(2,6-dimethylphenyl)-2,4-pentanediiminato)-bis(trimethylsillylmethylene)chromium(III)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 482323-03-5,604806-75-9
[CH(C(methyl)N(2,6-dimethylphenyl))₂Li]

: 635683-83-9
[(N,N'-bis(2,6-dimethylphenyl)-2,4-pentanediiminato)-bis(trimethylsillylmethylene)chromium(III)]

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: diethyl ether

In tetrahydrofuran; diethyl ether;
DOI:10.1021/ja043877x

Reference yield: 95.0%

: 635683-83-9
[(N,N'-bis(2,6-dimethylphenyl)-2,4-pentanediiminato)-bis(trimethylsillylmethylene)chromium(III)]

: 1333-74-0
hydrogen

: [((N,N'-bis(2,6-dimethylphenyl)-2,4-pentanediiminato)chromium(III))2(μ-trimethylsilylmethylene)(μ-H)]

Guidance literature:: In pentane; soln. of complex treated with H2 (1 atm) at room temp., stirred overnight, evapd.; extd. (Et2O), stored at -30°C, crystd. elem. anal.;
DOI:10.1039/b301943h

Reference yield:

: Brookhart's acid

: 635683-83-9
[(N,N'-bis(2,6-dimethylphenyl)-2,4-pentanediiminato)-bis(trimethylsillylmethylene)chromium(III)]

: 847153-55-3
[(2,4-pentane-N,N'-bis(2,6-dimethylphenyl)ketiminato)Cr(OEt₂)(CH₂SiMe₃)][B(3,5-(CF₃)2C₆H₃)4]

Guidance literature:: In dichloromethane; byproducts: SiMe4; Cr complex was treated with B compd. in CH2Cl2; recrystd. (CH2Cl2/pentane);
DOI:10.1021/ja043877x