3-(4-methoxyphenyl)-5-phenylisothiazole

Base Information

Chemical Name:3-(4-methoxyphenyl)-5-phenylisothiazole
CAS No.:68004-08-0
Molecular Formula:C₁₆H₁₃NOS
Molecular Weight:267.351
Hs Code.:

Synonyms:3-(4-methoxyphenyl)-5-phenylisothiazole

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Chemical Property of 3-(4-methoxyphenyl)-5-phenylisothiazole

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Technology Process of 3-(4-methoxyphenyl)-5-phenylisothiazole

There total 6 articles about 3-(4-methoxyphenyl)-5-phenylisothiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: (E)-1-(4-methoxyphenyl)-3-phenylprop-2-yn-1-one O-methyl oxime

: 68004-08-0
3-(4-methoxyphenyl)-5-phenylisothiazole

Guidance literature:: With sodium sulfide; water; sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 90 ℃; Schlenk technique;
DOI:10.1021/acs.joc.0c02286

Reference yield:

: 4-(4-methoxyphenyl)-6-phenyl-2H-1,3-thiazine-2-thione

: 68004-08-0
3-(4-methoxyphenyl)-5-phenylisothiazole

Guidance literature:: With iodine; In methanol; at 70 ℃; for 0.5h; Schlenk technique; Sealed tube; Inert atmosphere;
DOI:10.1021/acs.orglett.9b04437

Reference yield:

: 16616-43-6
1-(4-methoxy-phenyl)-3-phenyl-propynone

: 68004-08-0
3-(4-methoxyphenyl)-5-phenylisothiazole

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / 20 h / 100 °C / Schlenk technique; Inert atmosphere; Sealed tube

2: iodine / methanol / 0.5 h / 70 °C / Schlenk technique; Sealed tube; Inert atmosphere

With iodine; acetic acid; In methanol;
DOI:10.1021/acs.orglett.9b04437