(3S,4S)-8-[N-(2-chlorobenzyloxycarbonyl)amino]-4-[N-(2-nitrophenylsulfonyl)amino]oct-1-ene-3-ol

Base Information

Chemical Name:(3S,4S)-8-[N-(2-chlorobenzyloxycarbonyl)amino]-4-[N-(2-nitrophenylsulfonyl)amino]oct-1-ene-3-ol
CAS No.:1186125-41-6
Molecular Formula:C₂₂H₂₆ClN₃O₇S
Molecular Weight:511.983
Hs Code.:

Synonyms:(3S,4S)-8-[N-(2-chlorobenzyloxycarbonyl)amino]-4-[N-(2-nitrophenylsulfonyl)amino]oct-1-ene-3-ol

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Chemical Property of (3S,4S)-8-[N-(2-chlorobenzyloxycarbonyl)amino]-4-[N-(2-nitrophenylsulfonyl)amino]oct-1-ene-3-ol

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Technology Process of (3S,4S)-8-[N-(2-chlorobenzyloxycarbonyl)amino]-4-[N-(2-nitrophenylsulfonyl)amino]oct-1-ene-3-ol

There total 2 articles about (3S,4S)-8-[N-(2-chlorobenzyloxycarbonyl)amino]-4-[N-(2-nitrophenylsulfonyl)amino]oct-1-ene-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₂₃ClN₂O₃

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 1186125-41-6
(3S,4S)-8-[N-(2-chlorobenzyloxycarbonyl)amino]-4-[N-(2-nitrophenylsulfonyl)amino]oct-1-ene-3-ol

Guidance literature:: With 2,4,6-trimethyl-pyridine; In chloroform; at 0 - 20 ℃; for 1.5h;
DOI:10.1039/b907983a

Reference yield:

: 1186125-39-2
C₂₁H₃₁ClN₂O₅

: 1186125-41-6
(3S,4S)-8-[N-(2-chlorobenzyloxycarbonyl)amino]-4-[N-(2-nitrophenylsulfonyl)amino]oct-1-ene-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; water / 1,4-dioxane / 2 h / 0 - 20 °C

2: 2,4,6-trimethyl-pyridine / chloroform / 1.5 h / 0 - 20 °C

With 2,4,6-trimethyl-pyridine; hydrogenchloride; water; In 1,4-dioxane; chloroform;
DOI:10.1039/b907983a

Reference yield: 84.0%

: 1186125-41-6
(3S,4S)-8-[N-(2-chlorobenzyloxycarbonyl)amino]-4-[N-(2-nitrophenylsulfonyl)amino]oct-1-ene-3-ol

: 1186125-42-7
(3R,4S)-8-[N-(2-chlorobenzyloxycarbonyl)amino]-3,4-[N-(2-nitrophenylsulfonyl)epimino]oct-1-ene

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; toluene; at 0 - 20 ℃; for 4h; Inert atmosphere;
DOI:10.1039/b907983a