(3R,4S)-8-[N-(2-chlorobenzyloxycarbonyl)amino]-3,4-[N-(2-nitrophenylsulfonyl)epimino]oct-1-ene

Base Information

Chemical Name:(3R,4S)-8-[N-(2-chlorobenzyloxycarbonyl)amino]-3,4-[N-(2-nitrophenylsulfonyl)epimino]oct-1-ene
CAS No.:1186125-42-7
Molecular Formula:C₂₂H₂₄ClN₃O₆S
Molecular Weight:493.968
Hs Code.:

Synonyms:(3R,4S)-8-[N-(2-chlorobenzyloxycarbonyl)amino]-3,4-[N-(2-nitrophenylsulfonyl)epimino]oct-1-ene

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Chemical Property of (3R,4S)-8-[N-(2-chlorobenzyloxycarbonyl)amino]-3,4-[N-(2-nitrophenylsulfonyl)epimino]oct-1-ene

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Technology Process of (3R,4S)-8-[N-(2-chlorobenzyloxycarbonyl)amino]-3,4-[N-(2-nitrophenylsulfonyl)epimino]oct-1-ene

There total 4 articles about (3R,4S)-8-[N-(2-chlorobenzyloxycarbonyl)amino]-3,4-[N-(2-nitrophenylsulfonyl)epimino]oct-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1186125-41-6
(3S,4S)-8-[N-(2-chlorobenzyloxycarbonyl)amino]-4-[N-(2-nitrophenylsulfonyl)amino]oct-1-ene-3-ol

: 1186125-42-7
(3R,4S)-8-[N-(2-chlorobenzyloxycarbonyl)amino]-3,4-[N-(2-nitrophenylsulfonyl)epimino]oct-1-ene

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; toluene; at 0 - 20 ℃; for 4h; Inert atmosphere;
DOI:10.1039/b907983a

Reference yield:

: C₁₆H₂₃ClN₂O₃

: 1186125-42-7
(3R,4S)-8-[N-(2-chlorobenzyloxycarbonyl)amino]-3,4-[N-(2-nitrophenylsulfonyl)epimino]oct-1-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 2,4,6-trimethyl-pyridine / chloroform / 1.5 h / 0 - 20 °C

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran; toluene / 4 h / 0 - 20 °C / Inert atmosphere

With 2,4,6-trimethyl-pyridine; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; chloroform; toluene; 2: Mitsunobu reaction;
DOI:10.1039/b907983a

Reference yield:

: 1186125-39-2
C₂₁H₃₁ClN₂O₅

: 1186125-42-7
(3R,4S)-8-[N-(2-chlorobenzyloxycarbonyl)amino]-3,4-[N-(2-nitrophenylsulfonyl)epimino]oct-1-ene

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; water / 1,4-dioxane / 2 h / 0 - 20 °C

2: 2,4,6-trimethyl-pyridine / chloroform / 1.5 h / 0 - 20 °C

3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran; toluene / 4 h / 0 - 20 °C / Inert atmosphere

With 2,4,6-trimethyl-pyridine; hydrogenchloride; di-isopropyl azodicarboxylate; water; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; chloroform; toluene; 3: Mitsunobu reaction;
DOI:10.1039/b907983a