(Z)-1-Cyclohexyl-3-(dimethylphenylsilyl)prop-2-enol tert-butyldimethylsilyl ether

Base Information

Chemical Name:(Z)-1-Cyclohexyl-3-(dimethylphenylsilyl)prop-2-enol tert-butyldimethylsilyl ether
CAS No.:159616-10-1
Molecular Formula:C₂₃H₄₀OSi₂
Molecular Weight:388.741
Hs Code.:

Synonyms:(Z)-1-Cyclohexyl-3-(dimethylphenylsilyl)prop-2-enol tert-butyldimethylsilyl ether

Suppliers and Price of (Z)-1-Cyclohexyl-3-(dimethylphenylsilyl)prop-2-enol tert-butyldimethylsilyl ether

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-1-Cyclohexyl-3-(dimethylphenylsilyl)prop-2-enol tert-butyldimethylsilyl ether

Chemical Property:

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Technology Process of (Z)-1-Cyclohexyl-3-(dimethylphenylsilyl)prop-2-enol tert-butyldimethylsilyl ether

There total 4 articles about (Z)-1-Cyclohexyl-3-(dimethylphenylsilyl)prop-2-enol tert-butyldimethylsilyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 159616-10-1
(Z)-1-Cyclohexyl-3-(dimethylphenylsilyl)prop-2-enol tert-butyldimethylsilyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / imidazole / 48 h / Ambient temperature

2: 1.) DIBAL-H, 2.) n-BuLi / 1.) ether, reflux, 2 h, 2.) ether, hexane, 0 deg C, 10 min; r.t., 50 min

With 1H-imidazole; n-butyllithium; diisobutylaluminium hydride;
DOI:10.1021/jo00100a023

Reference yield:

: 130708-18-8
1-Cyclohexyl-3-(dimethylphenylsilyl)prop-2-ynol

: 159616-10-1
(Z)-1-Cyclohexyl-3-(dimethylphenylsilyl)prop-2-enol tert-butyldimethylsilyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / imidazole / 48 h / Ambient temperature

2: 1.) DIBAL-H, 2.) n-BuLi / 1.) ether, reflux, 2 h, 2.) ether, hexane, 0 deg C, 10 min; r.t., 50 min

With 1H-imidazole; n-butyllithium; diisobutylaluminium hydride;
DOI:10.1021/jo00100a023

Reference yield:

: 159616-09-8
1-Cyclohexyl-3-(dimethylphenylsilyl)prop-2-ynol tert-butyldimethylsilyl ether

: 159616-10-1
(Z)-1-Cyclohexyl-3-(dimethylphenylsilyl)prop-2-enol tert-butyldimethylsilyl ether

Guidance literature:: With n-butyllithium; diisobutylaluminium hydride; Yield given. Multistep reaction; 1.) ether, reflux, 2 h, 2.) ether, hexane, 0 deg C, 10 min; r.t., 50 min;
DOI:10.1021/jo00100a023