1,5-dicyano-3,7-bis[(3-cyano-4,7-dihydro-4,7-ethano-2H-isoindolyl)(4-tert-butylphenyl)methyl]-4,8-dihydro-4,8-ethanopyrrolo-[3,4-f]isoindole

Base Information

Chemical Name:1,5-dicyano-3,7-bis[(3-cyano-4,7-dihydro-4,7-ethano-2H-isoindolyl)(4-tert-butylphenyl)methyl]-4,8-dihydro-4,8-ethanopyrrolo-[3,4-f]isoindole
CAS No.:1454257-51-2
Molecular Formula:C₅₈H₅₄N₈
Molecular Weight:863.12
Hs Code.:

Synonyms:1,5-dicyano-3,7-bis[(3-cyano-4,7-dihydro-4,7-ethano-2H-isoindolyl)(4-tert-butylphenyl)methyl]-4,8-dihydro-4,8-ethanopyrrolo-[3,4-f]isoindole

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Chemical Property of 1,5-dicyano-3,7-bis[(3-cyano-4,7-dihydro-4,7-ethano-2H-isoindolyl)(4-tert-butylphenyl)methyl]-4,8-dihydro-4,8-ethanopyrrolo-[3,4-f]isoindole

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Technology Process of 1,5-dicyano-3,7-bis[(3-cyano-4,7-dihydro-4,7-ethano-2H-isoindolyl)(4-tert-butylphenyl)methyl]-4,8-dihydro-4,8-ethanopyrrolo-[3,4-f]isoindole

There total 1 articles about 1,5-dicyano-3,7-bis[(3-cyano-4,7-dihydro-4,7-ethano-2H-isoindolyl)(4-tert-butylphenyl)methyl]-4,8-dihydro-4,8-ethanopyrrolo-[3,4-f]isoindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1189-71-5
isocyanate de chlorosulfonyle

: 1454257-50-1
3,7-bis[(4,7-dihydro-4,7-ethano-2H-isoindolyl)(4-tert-butyl-phenyl)methyl]-4,8-dihydro-4,8-ethanopyrrolo[3,4-f]isoindole

: 1454257-51-2
1,5-dicyano-3,7-bis[(3-cyano-4,7-dihydro-4,7-ethano-2H-isoindolyl)(4-tert-butylphenyl)methyl]-4,8-dihydro-4,8-ethanopyrrolo-[3,4-f]isoindole

Guidance literature:: In N,N-dimethyl-formamide; acetonitrile; at -50 - 20 ℃; Inert atmosphere;
DOI:10.1039/c3ob41996g

Reference yield: 61.0%

: 109-63-7
boron trifluoride diethyl etherate

: 1454257-51-2
1,5-dicyano-3,7-bis[(3-cyano-4,7-dihydro-4,7-ethano-2H-isoindolyl)(4-tert-butylphenyl)methyl]-4,8-dihydro-4,8-ethanopyrrolo-[3,4-f]isoindole

: 9,18-di(4-tert-butylphenyl)-5,7,14,16-tetracyano-1,4,8,10,13,17-hexahydro-1,4:8,17:10,13-triethano-6,15-dibora-5a,6a,14a,15a-tetraaza-s-indaceno[2,3-b:6,7-b′]difluorene

Guidance literature:: 1,5-dicyano-3,7-bis[(3-cyano-4,7-dihydro-4,7-ethano-2H-isoindolyl)(4-tert-butylphenyl)methyl]-4,8-dihydro-4,8-ethanopyrrolo-[3,4-f]isoindole; With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In toluene; at 20 ℃; for 1h; Darkness;

With triethylamine; In toluene; for 0.166667h; Darkness;

boron trifluoride diethyl etherate; In toluene; at 80 ℃; Darkness;
DOI:10.1039/c3ob41996g