5-aminomethyl-3-phenyl-2-trifluoromethyl-pyrazole[1,5-a]pyrimidin-7(4H)-one

Base Information

Chemical Name:5-aminomethyl-3-phenyl-2-trifluoromethyl-pyrazole[1,5-a]pyrimidin-7(4H)-one
CAS No.:1259537-05-7
Molecular Formula:C₁₄H₁₁F₃N₄O
Molecular Weight:308.263
Hs Code.:

Synonyms:5-aminomethyl-3-phenyl-2-trifluoromethyl-pyrazole[1,5-a]pyrimidin-7(4H)-one

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Chemical Property of 5-aminomethyl-3-phenyl-2-trifluoromethyl-pyrazole[1,5-a]pyrimidin-7(4H)-one

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Technology Process of 5-aminomethyl-3-phenyl-2-trifluoromethyl-pyrazole[1,5-a]pyrimidin-7(4H)-one

There total 5 articles about 5-aminomethyl-3-phenyl-2-trifluoromethyl-pyrazole[1,5-a]pyrimidin-7(4H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₁₃F₃N₄O₃

: 1259537-05-7
5-aminomethyl-3-phenyl-2-trifluoromethyl-pyrazole[1,5-a]pyrimidin-7(4H)-one

Guidance literature:: With hydrazine hydrate; In ethanol; for 0.5h; Reflux;

Reference yield:

: 1259536-96-3
C₁₀H₅F₃NO^(1-)*Na⁽¹⁺⁾

: 1259537-05-7
5-aminomethyl-3-phenyl-2-trifluoromethyl-pyrazole[1,5-a]pyrimidin-7(4H)-one

Guidance literature:: Multi-step reaction with 4 steps

1: hydrazinium sulfate; carbonic acid dimethyl ester / 12 h / 80 °C

2: acetic acid / 4 h / Reflux

3: N,N-dimethyl-formamide / 8 h / 100 °C

4: hydrazine hydrate / ethanol / 0.5 h / Reflux

With hydrazine hydrate; acetic acid; carbonic acid dimethyl ester; hydrazinium sulfate; In ethanol; N,N-dimethyl-formamide;

Reference yield:

: 140-29-4
phenylacetonitrile

: 1259537-05-7
5-aminomethyl-3-phenyl-2-trifluoromethyl-pyrazole[1,5-a]pyrimidin-7(4H)-one

Guidance literature:: Multi-step reaction with 5 steps

1: sodium ethanolate / ethanol / 2 h / Reflux

2: hydrazinium sulfate; carbonic acid dimethyl ester / 12 h / 80 °C

3: acetic acid / 4 h / Reflux

4: N,N-dimethyl-formamide / 8 h / 100 °C

5: hydrazine hydrate / ethanol / 0.5 h / Reflux

With hydrazine hydrate; sodium ethanolate; acetic acid; carbonic acid dimethyl ester; hydrazinium sulfate; In ethanol; N,N-dimethyl-formamide;