methyl 2-methyl-4-({[(4S)-2,2,5,5-tetramethyl-1,3-dioxolan-4-yl]methyl}oxy)benzoate

Base Information

Chemical Name:methyl 2-methyl-4-({[(4S)-2,2,5,5-tetramethyl-1,3-dioxolan-4-yl]methyl}oxy)benzoate
CAS No.:1093988-65-8
Molecular Formula:C₁₇H₂₄O₅
Molecular Weight:308.375
Hs Code.:

Synonyms:methyl 2-methyl-4-({[(4S)-2,2,5,5-tetramethyl-1,3-dioxolan-4-yl]methyl}oxy)benzoate

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Chemical Property of methyl 2-methyl-4-({[(4S)-2,2,5,5-tetramethyl-1,3-dioxolan-4-yl]methyl}oxy)benzoate

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Technology Process of methyl 2-methyl-4-({[(4S)-2,2,5,5-tetramethyl-1,3-dioxolan-4-yl]methyl}oxy)benzoate

There total 5 articles about methyl 2-methyl-4-({[(4S)-2,2,5,5-tetramethyl-1,3-dioxolan-4-yl]methyl}oxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 57556-31-7
4-hydroxy-2-methylbenzoic acid methyl ester

: 37504-94-2
p-Toluolsulfonsaeure-<((4S)-2,2,5,5-tetramethyl-1,3-dioxolan-4-yl)methyl>ester

: 1093988-65-8
methyl 2-methyl-4-({[(4S)-2,2,5,5-tetramethyl-1,3-dioxolan-4-yl]methyl}oxy)benzoate

Guidance literature:: With 1-methyl-pyrrolidin-2-one; potassium carbonate; at 150 ℃; for 8h;

Reference yield:

: 578-39-2
4-hydroxy-2-methylbenzoic acid

: 1093988-65-8
methyl 2-methyl-4-({[(4S)-2,2,5,5-tetramethyl-1,3-dioxolan-4-yl]methyl}oxy)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydrogencarbonate / N,N-dimethyl-formamide / 3 h / 20 - 40 °C

1.2: 40 °C

2.1: 1-methyl-pyrrolidin-2-one; potassium carbonate / 8 h / 150 °C

With 1-methyl-pyrrolidin-2-one; potassium carbonate; potassium hydrogencarbonate; In N,N-dimethyl-formamide;

Reference yield:

: 86562-71-2
2-<(S)-2,2-dimethyl-1,3-dioxolane-4-yl>-2-propanol

: 1093988-65-8
methyl 2-methyl-4-({[(4S)-2,2,5,5-tetramethyl-1,3-dioxolan-4-yl]methyl}oxy)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridinium p-toluenesulfonate / methanol; water / Reflux

2.1: pyridine / 72 h / -20 °C / Inert atmosphere

2.2: 20 °C

3.1: toluene-4-sulfonic acid / tetrahydrofuran / 20 °C

3.2: 20 °C

4.1: 1-methyl-pyrrolidin-2-one; potassium carbonate / 8 h / 150 °C

With pyridine; 1-methyl-pyrrolidin-2-one; pyridinium p-toluenesulfonate; potassium carbonate; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; water;