N-(1-(4-(benzyloxy)phenyl)-4-(4-methoxyphenyl)but-3-yn-2-yl)-N-methylcyanamide

Base Information

• Chemical Name: N-(1-(4-(benzyloxy)phenyl)-4-(4-methoxyphenyl)but-3-yn-2-yl)-N-methylcyanamide
• CAS No.: 1161831-09-9
• Molecular Formula: C₂₆H₂₄N₂O₂
• Molecular Weight: 396.489

Synonyms:N-(1-(4-(benzyloxy)phenyl)-4-(4-methoxyphenyl)but-3-yn-2-yl)-N-methylcyanamide

Chemical Property of N-(1-(4-(benzyloxy)phenyl)-4-(4-methoxyphenyl)but-3-yn-2-yl)-N-methylcyanamide

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Technology Process of N-(1-(4-(benzyloxy)phenyl)-4-(4-methoxyphenyl)but-3-yn-2-yl)-N-methylcyanamide

There total 1 articles about N-(1-(4-(benzyloxy)phenyl)-4-(4-methoxyphenyl)but-3-yn-2-yl)-N-methylcyanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

bromocyane (506-68-3) + 1-(4-(benzyloxy)phenyl)-N-(4-methoxybenzyl)-4-(4-methoxyphenyl)-N-methylbut-3-yn-2-amine (1161831-03-3) → N-(1-(4-(benzyloxy)phenyl)-4-(4-methoxyphenyl)but-3-yn-2-yl)-N-methylcyanamide (1161831-09-9)

Guidance literature:

With potassium carbonate; In 1,4-dioxane; dichloromethane; at 20 ℃;

DOI:10.1002/anie.200900160

Reference yield: 89.0%

N-(1-(4-(benzyloxy)phenyl)-4-(4-methoxyphenyl)but-3-yn-2-yl)-N-methylcyanamide (1161831-09-9) + diallylamine (124-02-7) → N,N-diallyl-5-(4-(benzyloxy)benzyl)-4-(4-methoxybenzyl)-1-methyl-1H-imidazol-2-amine (1161831-18-0)

Guidance literature:

With lanthanum(lll) triflate; at 95 ℃; for 24h; Neat (no solvent);

DOI:10.1002/anie.200900160

Reference yield: 87.0%

N-(1-(4-(benzyloxy)phenyl)-4-(4-methoxyphenyl)but-3-yn-2-yl)-N-methylcyanamide (1161831-09-9) + thiophenol (108-98-5) → 5-(4-(benzyloxy)benzyl)-4-(4-methoxybenzyl)-1-methyl-2-(phenylthio)-1H-imidazole (1202223-18-4)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In isopropyl alcohol; at 120 ℃; for 24h;

DOI:10.1021/jo902326d

upstream raw materials:

bromocyane

1-(4-(benzyloxy)phenyl)-N-(4-methoxybenzyl)-4-(4-methoxyphenyl)-N-methylbut-3-yn-2-amine

Downstream raw materials:

8-(5-(4-(benzyloxy)benzyl)-4-(4-methoxybenzyl)-1-methyl-1H-imidazol-2-yl)1,4-dioxa-8-azaspiro-[4,5]decane

N,N-diallyl-5-(4-(benzyloxy)benzyl)-4-(4-methoxybenzyl)-1-methyl-1H-imidazol-2-amine

4-(5-(4-(benzyloxy)benzyl)-4-(4-methoxybenzyl)-1-methyl-1H-imidazol-2-ylthio)phenol

5-(4-(benzyloxy)benzyl)-4-(4-methoxybenzyl)-2-(4-methoxybenzylthio)-1-methyl-1H-imidazole

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