N-(4-Bromo-2-chloro-6-trifluoromethyl-phenyl)-3-cyclopentyl-propionamide

Base Information

• Chemical Name: N-(4-Bromo-2-chloro-6-trifluoromethyl-phenyl)-3-cyclopentyl-propionamide
• CAS No.: 1009344-69-7
• Molecular Formula: C₁₅H₁₆BrClF₃NO
• Molecular Weight: 398.65

Synonyms:N-(4-Bromo-2-chloro-6-trifluoromethyl-phenyl)-3-cyclopentyl-propionamide

Chemical Property of N-(4-Bromo-2-chloro-6-trifluoromethyl-phenyl)-3-cyclopentyl-propionamide

Chemical Property:

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Technology Process of N-(4-Bromo-2-chloro-6-trifluoromethyl-phenyl)-3-cyclopentyl-propionamide

There total 1 articles about N-(4-Bromo-2-chloro-6-trifluoromethyl-phenyl)-3-cyclopentyl-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-bromo-2-chloro-6-(trifluoromethyl)aniline (870703-71-2) + cyclopentanepropanoyl chloride (104-97-2) → N-(4-Bromo-2-chloro-6-trifluoromethyl-phenyl)-3-cyclopentyl-propionamide (1009344-69-7)

Guidance literature:

In acetonitrile; at 20 ℃;

Reference yield: 28.0%

1,2,3,4-tetrahydroisoquinoline (91-21-4) + N-(4-Bromo-2-chloro-6-trifluoromethyl-phenyl)-3-cyclopentyl-propionamide (1009344-69-7) → N-(2-chloro-4-(3,4-dihydroisoquinolin-2(1H)-yl)-6-(trifluoromethyl)phenyl)-3-cyclopentylpropanamide (1009344-21-1)

Guidance literature:

With potassium tert-butylate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; DavePhos; In toluene; at 90 ℃;

Reference yield:

N-(4-Bromo-2-chloro-6-trifluoromethyl-phenyl)-3-cyclopentyl-propionamide (1009344-69-7) + 6-fluoro-1,2,3,4-tetrahydroisoquinoline hydrochloride (799274-08-1) → N-[2-Chloro-4-(6-fluoro-3,4-dihydro-1H-isoquinolin-2-yl)-6-trifluoromethyl-phenyl]-3-cyclopentyl-propionamide (1009344-27-7)

Guidance literature:

With potassium tert-butylate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; DavePhos; In toluene; at 90 ℃;

upstream raw materials:

4-bromo-2-chloro-6-(trifluoromethyl)aniline

cyclopentanepropanoyl chloride

Downstream raw materials:

N-(2-chloro-4-(3,4-dihydroisoquinolin-2(1H)-yl)-6-(trifluoromethyl)phenyl)-3-cyclopentylpropanamide

N-[2-Chloro-4-(6-fluoro-3,4-dihydro-1H-isoquinolin-2-yl)-6-trifluoromethyl-phenyl]-3-cyclopentyl-propionamide

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