C₁₁H₁₆O

Base Information

• Chemical Name: C₁₁H₁₆O
• CAS No.: 1030239-96-3
• Molecular Formula: C₁₁H₁₆O
• Molecular Weight: 164.247
• Mol file: 1030239-96-3.mol

Synonyms:C₁₁H₁₆O

Chemical Property of C₁₁H₁₆O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of C₁₁H₁₆O

There total 1 articles about C₁₁H₁₆O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

cyclohept-1-en-1-yl trifluoromethanesulfonate (28075-51-6) + carbon monoxide (201230-82-2) + isopropenylmagnesium bromide (13291-18-4) → C11H16O (1030239-96-3) + 2,3-dimethyl-buta-1,3-diene (513-81-5)

Guidance literature:

isopropenylmagnesium bromide; With zinc dibromide; In tetrahydrofuran; at 20 ℃;

cyclohept-1-en-1-yl trifluoromethanesulfonate; carbon monoxide; With zinc dibromide; nickel dichloride; In tetrahydrofuran; dimethyl sulfoxide; at 50 ℃; for 0.333333h; under 760.051 Torr; Further stages.;

DOI:10.1016/j.tetlet.2008.03.035

upstream raw materials:

cyclohept-1-en-1-yl trifluoromethanesulfonate

carbon monoxide

isopropenylmagnesium bromide

Refernces