C₃₁H₄₁N₃O₅

Base Information

Chemical Name:C₃₁H₄₁N₃O₅
CAS No.:1294006-96-4
Molecular Formula:C₃₁H₄₁N₃O₅
Molecular Weight:535.684
Hs Code.:

C<sub>31</sub>H<sub>41</sub>N<sub>3</sub>O<sub>5</sub>

Synonyms:C₃₁H₄₁N₃O₅

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Chemical Property of C₃₁H₄₁N₃O₅

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Technology Process of C₃₁H₄₁N₃O₅

There total 8 articles about C₃₁H₄₁N₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1294006-95-3
C₁₉H₂₇N₃O₃

: 131423-64-8
benzyl (R)-4-methyl-2-(trifluoromethylsulfonyloxy)pentanoate

: 1294006-96-4
C₃₁H₄₁N₃O₅

Guidance literature:: With 2,6-dimethylpyridine; In 1,2-dichloro-ethane; for 24h; Reflux;
DOI:10.1039/c0ob01115k

Reference yield:

: 162955-48-8,397246-12-7
[(1S)-4-hydroxy-1-(hydroxymethyl)butyl]carbamic acid tert-butyl ester

: 1294006-96-4
C₃₁H₄₁N₃O₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: boron trifluoride diethyl etherate / acetone / 24 h / 20 °C

1.2: pH 6 - 7

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

2.2: 1 h / -78 - 20 °C

3.1: 1,4-diaza-bicyclo[2.2.2]octane; palladium diacetate / N,N-dimethyl-formamide / 12 h / 80 °C / Inert atmosphere

4.1: palladium 10% on activated carbon; hydrogen / methanol / 20 °C / 3040.2 Torr

5.1: 2,6-dimethylpyridine / 1,2-dichloro-ethane / 24 h / Reflux

With 1,4-diaza-bicyclo[2.2.2]octane; 2,6-dimethylpyridine; oxalyl dichloride; palladium 10% on activated carbon; boron trifluoride diethyl etherate; hydrogen; palladium diacetate; dimethyl sulfoxide; In methanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone; 2.1: Swern oxidation / 2.2: Swern oxidation;
DOI:10.1039/c0ob01115k

Reference yield:

: 1294006-88-4
C₁₉H₂₅N₃O₅

: 1294006-96-4
C₃₁H₄₁N₃O₅

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 20 °C / 3040.2 Torr

2: 2,6-dimethylpyridine / 1,2-dichloro-ethane / 24 h / Reflux

With 2,6-dimethylpyridine; palladium 10% on activated carbon; hydrogen; In methanol; 1,2-dichloro-ethane;
DOI:10.1039/c0ob01115k