6-[4-(methyl 2,3,4-tri-O-benzyl-α-D-glucopyranosiduronylmethyl)-1H-1,2,3-triazol-1-yl]hexyl 3β-hydroxyolean-12-en-28-oate

Base Information

Chemical Name:6-[4-(methyl 2,3,4-tri-O-benzyl-α-D-glucopyranosiduronylmethyl)-1H-1,2,3-triazol-1-yl]hexyl 3β-hydroxyolean-12-en-28-oate
CAS No.:1161826-41-0
Molecular Formula:C₆₇H₉₁N₃O₁₀
Molecular Weight:1098.47
Hs Code.:

Synonyms:6-[4-(methyl 2,3,4-tri-O-benzyl-α-D-glucopyranosiduronylmethyl)-1H-1,2,3-triazol-1-yl]hexyl 3β-hydroxyolean-12-en-28-oate

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Chemical Property of 6-[4-(methyl 2,3,4-tri-O-benzyl-α-D-glucopyranosiduronylmethyl)-1H-1,2,3-triazol-1-yl]hexyl 3β-hydroxyolean-12-en-28-oate

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Technology Process of 6-[4-(methyl 2,3,4-tri-O-benzyl-α-D-glucopyranosiduronylmethyl)-1H-1,2,3-triazol-1-yl]hexyl 3β-hydroxyolean-12-en-28-oate

There total 5 articles about 6-[4-(methyl 2,3,4-tri-O-benzyl-α-D-glucopyranosiduronylmethyl)-1H-1,2,3-triazol-1-yl]hexyl 3β-hydroxyolean-12-en-28-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: propargyl (methyl 2,3,4-tri-O-benzyl-α-D-glucopyranosid)uronate

: 1161826-30-7
6-azidohexyl 3β-hydroxyolean-12-en-28-oate

: 1161826-41-0
6-[4-(methyl 2,3,4-tri-O-benzyl-α-D-glucopyranosiduronylmethyl)-1H-1,2,3-triazol-1-yl]hexyl 3β-hydroxyolean-12-en-28-oate

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In dichloromethane; water; at 20 ℃; for 8h;
DOI:10.1016/j.carres.2009.02.012

Reference yield:

: 235095-05-3
1-azido-6-bromohexane

: 1161826-41-0
6-[4-(methyl 2,3,4-tri-O-benzyl-α-D-glucopyranosiduronylmethyl)-1H-1,2,3-triazol-1-yl]hexyl 3β-hydroxyolean-12-en-28-oate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / dichloromethane; water / 8 h / 20 °C

With copper(ll) sulfate pentahydrate; potassium carbonate; sodium L-ascorbate; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2009.02.012

Reference yield:

: 508-02-1
Oleanolic acid

: 1161826-41-0
6-[4-(methyl 2,3,4-tri-O-benzyl-α-D-glucopyranosiduronylmethyl)-1H-1,2,3-triazol-1-yl]hexyl 3β-hydroxyolean-12-en-28-oate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / dichloromethane; water / 8 h / 20 °C

With copper(ll) sulfate pentahydrate; potassium carbonate; sodium L-ascorbate; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2009.02.012