o-tosylaminobenzaldehyde morpholinal

Base Information

• Chemical Name: o-tosylaminobenzaldehyde morpholinal
• CAS No.: 176214-83-8
• Molecular Formula: C₂₂H₂₉N₃O₄S
• Molecular Weight: 431.556

Synonyms:o-tosylaminobenzaldehyde morpholinal

Chemical Property of o-tosylaminobenzaldehyde morpholinal

Chemical Property:

Purity/Quality:

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Technology Process of o-tosylaminobenzaldehyde morpholinal

There total 1 articles about o-tosylaminobenzaldehyde morpholinal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

morpholine (110-91-8,99108-56-2) + N-(2-Formyl-phenyl)-4-methyl-benzenesulfonamide (6590-65-4) → o-tosylaminobenzaldehyde morpholinal (176214-83-8)

Guidance literature:

In isopropyl alcohol; 1.) boiling, 2.) 12 h;

DOI:10.1007/BF00696721

Reference yield: 94.4%

phenylacetylene (536-74-3) + o-tosylaminobenzaldehyde morpholinal (176214-83-8) → 4-Methyl-N-[2-(1-morpholin-4-yl-3-phenyl-prop-2-ynyl)-phenyl]-benzenesulfonamide (176214-89-4)

Guidance literature:

With copper(l) iodide; In acetonitrile; for 0.5h; Heating;

DOI:10.1007/BF00696721

Reference yield: 86.0%

cyanoacetic acid (372-09-8) + o-tosylaminobenzaldehyde morpholinal (176214-83-8) → acide amino-2 quinoleine carboxylique-3 (31407-29-1)

Guidance literature:

In acetonitrile; for 0.5h; Reflux;

DOI:10.1007/s11172-008-0065-0

upstream raw materials:

morpholine

N-(2-Formyl-phenyl)-4-methyl-benzenesulfonamide

Downstream raw materials:

4-Methyl-N-[2-(1-morpholin-4-yl-3-phenyl-prop-2-ynyl)-phenyl]-benzenesulfonamide

2-Phenylquinoline

NSC 19826

acide amino-2 quinoleine carboxylique-3

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