(1S,3R)-1,3-Dimethyl-3-(pyrrolidine-1-carbonyl)-cyclohexanecarboxylic acid cyanomethyl ester

Base Information

Chemical Name:(1S,3R)-1,3-Dimethyl-3-(pyrrolidine-1-carbonyl)-cyclohexanecarboxylic acid cyanomethyl ester
CAS No.:127183-15-7
Molecular Formula:C₁₆H₂₄N₂O₃
Molecular Weight:292.378
Hs Code.:

Synonyms:(1S,3R)-1,3-Dimethyl-3-(pyrrolidine-1-carbonyl)-cyclohexanecarboxylic acid cyanomethyl ester

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Chemical Property of (1S,3R)-1,3-Dimethyl-3-(pyrrolidine-1-carbonyl)-cyclohexanecarboxylic acid cyanomethyl ester

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Technology Process of (1S,3R)-1,3-Dimethyl-3-(pyrrolidine-1-carbonyl)-cyclohexanecarboxylic acid cyanomethyl ester

There total 7 articles about (1S,3R)-1,3-Dimethyl-3-(pyrrolidine-1-carbonyl)-cyclohexanecarboxylic acid cyanomethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121-91-5
isophthalic acid

: 127183-15-7
(1S,3R)-1,3-Dimethyl-3-(pyrrolidine-1-carbonyl)-cyclohexanecarboxylic acid cyanomethyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: H₂ / Rh/C

2: SOCl₂

4: LDA

6: Ac₂O

7: 1.) triethylamine / 1.) DMF

With thionyl chloride; hydrogen; acetic anhydride; triethylamine; lithium diisopropyl amide; Rh on carbon;
DOI:10.1021/jo00297a010

Reference yield:

: 3971-31-1
cyclohexane-1,3-dicarboxylic acid

: 127183-15-7
(1S,3R)-1,3-Dimethyl-3-(pyrrolidine-1-carbonyl)-cyclohexanecarboxylic acid cyanomethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: SOCl₂

3: LDA

5: Ac₂O

6: 1.) triethylamine / 1.) DMF

With thionyl chloride; acetic anhydride; triethylamine; lithium diisopropyl amide;
DOI:10.1021/jo00297a010

Reference yield:

: 27768-32-7,22605-66-9,46065-16-1
cyclohexane-1,3-dicarbonyl dichloride

: 127183-15-7
(1S,3R)-1,3-Dimethyl-3-(pyrrolidine-1-carbonyl)-cyclohexanecarboxylic acid cyanomethyl ester

Guidance literature:: Multi-step reaction with 5 steps

2: LDA

4: Ac₂O

5: 1.) triethylamine / 1.) DMF

With acetic anhydride; triethylamine; lithium diisopropyl amide;
DOI:10.1021/jo00297a010