N-{2-[3-Azido-2-(tert-butyl-dimethyl-silanyloxy)-propyl]-phenyl}-2,2,2-trifluoro-acetamide

Base Information

Chemical Name:N-{2-[3-Azido-2-(tert-butyl-dimethyl-silanyloxy)-propyl]-phenyl}-2,2,2-trifluoro-acetamide
CAS No.:132871-54-6
Molecular Formula:C₁₇H₂₅F₃N₄O₂Si
Molecular Weight:402.492
Hs Code.:

Synonyms:N-{2-[3-Azido-2-(tert-butyl-dimethyl-silanyloxy)-propyl]-phenyl}-2,2,2-trifluoro-acetamide

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Chemical Property of N-{2-[3-Azido-2-(tert-butyl-dimethyl-silanyloxy)-propyl]-phenyl}-2,2,2-trifluoro-acetamide

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Technology Process of N-{2-[3-Azido-2-(tert-butyl-dimethyl-silanyloxy)-propyl]-phenyl}-2,2,2-trifluoro-acetamide

There total 5 articles about N-{2-[3-Azido-2-(tert-butyl-dimethyl-silanyloxy)-propyl]-phenyl}-2,2,2-trifluoro-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 132871-53-5
N-[2-(3-Azido-2-hydroxy-propyl)-phenyl]-2,2,2-trifluoro-acetamide

: 18162-48-6
tert-butyldimethylsilyl chloride

: 132871-54-6
N-{2-[3-Azido-2-(tert-butyl-dimethyl-silanyloxy)-propyl]-phenyl}-2,2,2-trifluoro-acetamide

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 60 ℃;
DOI:10.1016/S0040-4039(00)97229-0

Reference yield:

: 589-09-3
N-allyl-N-phenylamine

: 132871-54-6
N-{2-[3-Azido-2-(tert-butyl-dimethyl-silanyloxy)-propyl]-phenyl}-2,2,2-trifluoro-acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: Aza-Claisen reaction

2: Na₂CO₃ / diethyl ether

3: MCPBA, Na₂CO₃ / CH₂Cl₂

4: NaN₃, NH₄Cl / H₂O; acetonitrile

5: 100 percent / imidazole / dimethylformamide / 60 °C

With 1H-imidazole; sodium azide; sodium carbonate; ammonium chloride; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4039(00)97229-0

Reference yield:

: 32704-22-6
2-allyl-phenylamine

: 132871-54-6
N-{2-[3-Azido-2-(tert-butyl-dimethyl-silanyloxy)-propyl]-phenyl}-2,2,2-trifluoro-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: Na₂CO₃ / diethyl ether

2: MCPBA, Na₂CO₃ / CH₂Cl₂

3: NaN₃, NH₄Cl / H₂O; acetonitrile

4: 100 percent / imidazole / dimethylformamide / 60 °C

With 1H-imidazole; sodium azide; sodium carbonate; ammonium chloride; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4039(00)97229-0