1-[p-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-10-[m-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-3,6-dioxaoctane

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Chemical Name:1-[p-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-10-[m-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-3,6-dioxaoctane
CAS No.:189118-57-8
Molecular Formula:C₈₀H₈₂O₁₂
Molecular Weight:1235.52
Hs Code.:

Synonyms:1-[p-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-10-[m-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-3,6-dioxaoctane

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Chemical Property of 1-[p-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-10-[m-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-3,6-dioxaoctane

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Technology Process of 1-[p-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-10-[m-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-3,6-dioxaoctane

There total 12 articles about 1-[p-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-10-[m-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-3,6-dioxaoctane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 189118-53-4
3-(2-{2-[2-(4-Trityl-phenoxy)-ethoxy]-ethoxy}-ethoxy)-phenol

: 189118-56-7
2-<2-<2-<4-<2-<2-<2-(4-triphenylmethylphenoxy)ethoxy>ethoxy>ethoxy>phenoxy>ethoxy>ethoxy>ethanoltosylate

: 189118-57-8
1-[p-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-10-[m-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-3,6-dioxaoctane

Guidance literature:: With potassium carbonate; lithium bromide; In acetonitrile; for 120h; Heating;
DOI:10.1021/jo9612584

Reference yield:

: 5197-62-6
2-[2-(chloroethoxy)ethoxy]ethanol

: 189118-57-8
1-[p-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-10-[m-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-3,6-dioxaoctane

Guidance literature:: Multi-step reaction with 7 steps

1: 84 percent / K₂CO₃ / acetonitrile / 72 h / Heating

2: 82 percent / triethylamine, 4-dimethylaminopyridine / CH₂Cl₂ / 4 h / 0 - 20 °C

3: 45 percent / K₂CO₃ / acetonitrile / 96 h / 80 °C

4: 95 percent / hydrogen / Pd/C / CH₂Cl₂; methanol / 15 h

5: 69 percent / K₂CO₃ / acetonitrile / 72 h / Heating

6: 41 percent / triethylamine, 4-dimethylaminopyridine / CH₂Cl₂ / 2 h / 0 °C

7: 71 percent / K₂CO₃, LiBr / acetonitrile / 120 h / Heating

With dmap; hydrogen; potassium carbonate; triethylamine; lithium bromide; palladium on activated charcoal; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/jo9612584

Reference yield:

: 103-16-2
4-Benzyloxyphenol

: 189118-57-8
1-[p-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-10-[m-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-3,6-dioxaoctane

Guidance literature:: Multi-step reaction with 7 steps

1: 84 percent / K₂CO₃ / acetonitrile / 72 h / Heating

2: 82 percent / triethylamine, 4-dimethylaminopyridine / CH₂Cl₂ / 4 h / 0 - 20 °C

3: 45 percent / K₂CO₃ / acetonitrile / 96 h / 80 °C

4: 95 percent / hydrogen / Pd/C / CH₂Cl₂; methanol / 15 h

5: 69 percent / K₂CO₃ / acetonitrile / 72 h / Heating

6: 41 percent / triethylamine, 4-dimethylaminopyridine / CH₂Cl₂ / 2 h / 0 °C

7: 71 percent / K₂CO₃, LiBr / acetonitrile / 120 h / Heating

With dmap; hydrogen; potassium carbonate; triethylamine; lithium bromide; palladium on activated charcoal; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/jo9612584