O-methyl N-[1-(4-methoxybenzyl)-2-chloroindol-3-ylcarbonyl]thiocarbamate

Base Information

Chemical Name:O-methyl N-[1-(4-methoxybenzyl)-2-chloroindol-3-ylcarbonyl]thiocarbamate
CAS No.:407630-93-7
Molecular Formula:C₁₉H₁₇ClN₂O₃S
Molecular Weight:388.875
Hs Code.:

Synonyms:O-methyl N-[1-(4-methoxybenzyl)-2-chloroindol-3-ylcarbonyl]thiocarbamate

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Chemical Property of O-methyl N-[1-(4-methoxybenzyl)-2-chloroindol-3-ylcarbonyl]thiocarbamate

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Technology Process of O-methyl N-[1-(4-methoxybenzyl)-2-chloroindol-3-ylcarbonyl]thiocarbamate

There total 4 articles about O-methyl N-[1-(4-methoxybenzyl)-2-chloroindol-3-ylcarbonyl]thiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 67-56-1
methanol

: 407630-89-1
1-(4-methoxybenzyl)-2-chloroindol-3-ylcarbonyl isothiocyanate

: 2-chloro-1-(4-methoxy-benzyl)-1H-indole-3-carboxylic acid methyl ester

: 407630-93-7
O-methyl N-[1-(4-methoxybenzyl)-2-chloroindol-3-ylcarbonyl]thiocarbamate

Guidance literature:: at 60 ℃; for 1h;
DOI:10.1016/S0040-4020(02)01124-9

Reference yield:

: 77655-47-1
1-(p-metossibenzil)-2-cloroindol-3-carbossialdeide

: 407630-93-7
O-methyl N-[1-(4-methoxybenzyl)-2-chloroindol-3-ylcarbonyl]thiocarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: 58 percent / KMnO₄ / acetone; H₂O / 20 °C

2: PCl₃ / benzene / 1 h / 85 - 90 °C

3: 29 percent / acetone / 1 h / 20 °C

4: 40 percent / 1 h / 60 °C

With potassium permanganate; phosphorus trichloride; In water; acetone; benzene;
DOI:10.1016/S0040-4020(02)01124-9

Reference yield:

: 407630-85-7
1-(4-methoxybenzyl)-2-chloroindole-3-carboxylic acid

: 407630-93-7
O-methyl N-[1-(4-methoxybenzyl)-2-chloroindol-3-ylcarbonyl]thiocarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: PCl₃ / benzene / 1 h / 85 - 90 °C

2: 29 percent / acetone / 1 h / 20 °C

3: 40 percent / 1 h / 60 °C

With phosphorus trichloride; In acetone; benzene;
DOI:10.1016/S0040-4020(02)01124-9