methyl (2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

Base Information

Chemical Name:methyl (2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside
CAS No.:1037510-20-5
Molecular Formula:C₆₂H₅₂O₁₈
Molecular Weight:1085.08
Hs Code.:

Synonyms:methyl (2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

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Chemical Property of methyl (2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

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Technology Process of methyl (2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

There total 2 articles about methyl (2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 34234-44-1,53182-61-9,88037-32-5,101194-17-6,120104-44-1,120104-49-6
methyl 2,3,4-tri-O-benzoyl-α-D-mannopyranoside

: 627466-64-2
2,3,4,6-tetra-O-benzoyl-D-glucopyranose

: 1037510-20-5
methyl (2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

Guidance literature:: 2,3,4,6-tetra-O-benzoyl-D-glucopyranose; With 3-fluorophthalic anhydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 0.25h; Molecular sieve;

methyl 2,3,4-tri-O-benzoyl-α-D-mannopyranoside; In dichloromethane; at 0 ℃; for 0.25h;

With trifluoromethylsulfonic anhydride; In dichloromethane; at 0 - 20 ℃; for 0.75h; stereoselective reaction;
DOI:10.1016/j.tetlet.2010.09.064

Reference yield:

: 34234-44-1,53182-61-9,88037-32-5,101194-17-6,120104-44-1,120104-49-6
methyl 2,3,4-tri-O-benzoyl-α-D-mannopyranoside

: 2592-58-7,3006-48-2,3006-49-3,13526-09-5,14679-57-3,22415-91-4,29884-70-6,41545-55-5,41545-56-6,41569-33-9,96996-90-6,121570-85-2,121570-86-3
1,2,3,4,6-penta-O-benzoyl-D-glucopyranoside

: 98-88-4
benzoyl chloride

: 1037510-20-5
methyl (2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

: methyl 6-O-(2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

Guidance literature:: methyl 2,3,4-tri-O-benzoyl-α-D-mannopyranoside; 1,2,3,4,6-penta-O-benzoyl-D-glucopyranoside; With methanesulfonic acid; In neat (no solvent); at 110 ℃; for 2h;

benzoyl chloride; With pyridine; at 20 ℃; for 2.5h; Overall yield = 30 percent; stereoselective reaction;
DOI:10.1002/ejoc.202101121