Technology Process of C21H34O4
There total 6 articles about C21H34O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 0 - 20 °C
2: pyridinium p-toluenesulfonate / dichloromethane / 12 h / 0 - 20 °C
With
lithium aluminium tetrahydride; pyridinium p-toluenesulfonate;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2011.05.151
- Guidance literature:
-
Multi-step reaction with 6 steps
1: (-)-diisopinocampheylborane; dihydrogen peroxide; sodium hydroxide / 168 h
2: pyridinium chlorochromate / dichloromethane / 3 h / 0 - 20 °C
3: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / 2 h / 0 - 20 °C
4: lithium diisopropyl amide / tetrahydrofuran / 5 h / -78 °C
5: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 0 - 20 °C
6: pyridinium p-toluenesulfonate / dichloromethane / 12 h / 0 - 20 °C
With
lithium aluminium tetrahydride; (-)-diisopinocampheylborane; dihydrogen peroxide; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; sodium hydroxide; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane;
3: Baeyer-Villiger oxidation;
DOI:10.1016/j.tetlet.2011.05.151
