2-{(3R,4R,5R)-3-[(Dimethyl-phenyl-silanyl)-methyl]-2,2-diisobutyl-5-octyl-[1,2]oxasilolan-4-yl}-ethanol

Base Information

• Chemical Name: 2-{(3R,4R,5R)-3-[(Dimethyl-phenyl-silanyl)-methyl]-2,2-diisobutyl-5-octyl-[1,2]oxasilolan-4-yl}-ethanol
• CAS No.: 170238-51-4
• Molecular Formula: C₃₀H₅₆O₂Si₂
• Molecular Weight: 504.944

Synonyms:2-{(3R,4R,5R)-3-[(Dimethyl-phenyl-silanyl)-methyl]-2,2-diisobutyl-5-octyl-[1,2]oxasilolan-4-yl}-ethanol

Chemical Property of 2-{(3R,4R,5R)-3-[(Dimethyl-phenyl-silanyl)-methyl]-2,2-diisobutyl-5-octyl-[1,2]oxasilolan-4-yl}-ethanol

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Technology Process of 2-{(3R,4R,5R)-3-[(Dimethyl-phenyl-silanyl)-methyl]-2,2-diisobutyl-5-octyl-[1,2]oxasilolan-4-yl}-ethanol

There total 2 articles about 2-{(3R,4R,5R)-3-[(Dimethyl-phenyl-silanyl)-methyl]-2,2-diisobutyl-5-octyl-[1,2]oxasilolan-4-yl}-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C30H54OSi2 → 2-{(3R,4R,5R)-3-[(Dimethyl-phenyl-silanyl)-methyl]-2,2-diisobutyl-5-octyl-[1,2]oxasilolan-4-yl}-ethanol (170238-51-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 1,1,3,3-tetramethylbutyl isocyanide, Pd(OAc)2 / toluene / Ambient temperature

2: 1.) RhCl(PPh₃)2, catecholborane, 2.) H₂O₂, NaOAc

With palladium diacetate; [RhCl(Ph₃P)2]; 1,1,3,3-tetramethylbutane isonitrile; dihydrogen peroxide; sodium acetate; benzo[1,3,2]dioxaborole; In toluene;

DOI:10.1021/ja00142a047

Reference yield:

(3R,4R,5R)-3-[(Dimethyl-phenyl-silanyl)-methyl]-2,2-diisobutyl-5-octyl-4-vinyl-[1,2]oxasilolane (170238-50-3) → 2-{(3R,4R,5R)-3-[(Dimethyl-phenyl-silanyl)-methyl]-2,2-diisobutyl-5-octyl-[1,2]oxasilolan-4-yl}-ethanol (170238-51-4)

Guidance literature:

With [RhCl(Ph₃P)2]; dihydrogen peroxide; sodium acetate; benzo[1,3,2]dioxaborole; Yield given. Multistep reaction;

DOI:10.1021/ja00142a047

Reference yield: 86.0%

trityl chloride (76-83-5) + 2-{(3R,4R,5R)-3-[(Dimethyl-phenyl-silanyl)-methyl]-2,2-diisobutyl-5-octyl-[1,2]oxasilolan-4-yl}-ethanol (170238-51-4) → (3R,4R,5R)-3-[(Dimethyl-phenyl-silanyl)-methyl]-2,2-diisobutyl-5-octyl-4-(2-trityloxy-ethyl)-[1,2]oxasilolane

Guidance literature:

With dmap; triethylamine; Ambient temperature;

DOI:10.1021/ja00142a047

upstream raw materials:

(3R,4R,5R)-3-[(Dimethyl-phenyl-silanyl)-methyl]-2,2-diisobutyl-5-octyl-4-vinyl-[1,2]oxasilolane

Downstream raw materials:

(2R,3R,4R)-3-(2-Trityloxy-ethyl)-dodecane-1,2,4-triol

tert-Butyl-[(4R,5R,6R)-2,2-dimethyl-6-octyl-5-(2-trityloxy-ethyl)-[1,3]dioxan-4-ylmethoxy]-diphenyl-silane

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