(3S,4S) 3-<(benzyloxycarbonyl)amino>-4-<(carbamoyloxy)methyl>-2-azetidinone

Base Information

Chemical Name:(3S,4S) 3-<(benzyloxycarbonyl)amino>-4-<(carbamoyloxy)methyl>-2-azetidinone
CAS No.:86334-65-8
Molecular Formula:C₁₃H₁₅N₃O₅
Molecular Weight:293.279
Hs Code.:

Synonyms:(3S,4S) 3-<(benzyloxycarbonyl)amino>-4-<(carbamoyloxy)methyl>-2-azetidinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,4S) 3-<(benzyloxycarbonyl)amino>-4-<(carbamoyloxy)methyl>-2-azetidinone

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Technology Process of (3S,4S) 3-<(benzyloxycarbonyl)amino>-4-<(carbamoyloxy)methyl>-2-azetidinone

There total 10 articles about (3S,4S) 3-<(benzyloxycarbonyl)amino>-4-<(carbamoyloxy)methyl>-2-azetidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 108636-64-2,108691-86-7
3,4-cis-3-benzyloxycarbonylamino-4-carbamoyloxymethyl-1-(1-carboxy-2-methylpropyl)-2-azetidinone

: 86334-65-8
(3S,4S) 3-<(benzyloxycarbonyl)amino>-4-<(carbamoyloxy)methyl>-2-azetidinone

Guidance literature:: With acetic acid; triethylamine; In acetic acid; at 20 - 30 ℃; anodic oxidation using a platinum anode-platinum cathode;
DOI:10.3987/R-1986-08-2273

Reference yield:

: 1189-71-5
isocyanate de chlorosulfonyle

: 99397-29-2
(3S,4S)-3-benzyloxycarbonylamino-4-hydroxymethyl-2-azetidinone

: 86334-65-8
(3S,4S) 3-<(benzyloxycarbonyl)amino>-4-<(carbamoyloxy)methyl>-2-azetidinone

Guidance literature:: With sodium sulfite; In dichloromethane;

Reference yield:

: [(2S,3S)-2-(2-Chloro-acetylcarbamoyloxymethyl)-4-oxo-azetidin-3-yl]-carbamic acid benzyl ester

: 86334-65-8
(3S,4S) 3-<(benzyloxycarbonyl)amino>-4-<(carbamoyloxy)methyl>-2-azetidinone

Guidance literature:: With sodium N-methyldithiocarbamate; In dichloromethane; water; N,N-dimethyl-formamide; for 4h; Yield given; Ambient temperature;
DOI:10.1016/S0040-4020(01)89308-X