(S)-2-[5-(4-Chloro-phenylcarbamoyl)-thiophene-3-sulfonylamino]-4-methyl-pentanoic acid

Base Information

Chemical Name:(S)-2-[5-(4-Chloro-phenylcarbamoyl)-thiophene-3-sulfonylamino]-4-methyl-pentanoic acid
CAS No.:208775-93-3
Molecular Formula:C₁₇H₁₉ClN₂O₅S₂
Molecular Weight:430.933
Hs Code.:

Synonyms:(S)-2-[5-(4-Chloro-phenylcarbamoyl)-thiophene-3-sulfonylamino]-4-methyl-pentanoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-[5-(4-Chloro-phenylcarbamoyl)-thiophene-3-sulfonylamino]-4-methyl-pentanoic acid

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Technology Process of (S)-2-[5-(4-Chloro-phenylcarbamoyl)-thiophene-3-sulfonylamino]-4-methyl-pentanoic acid

There total 1 articles about (S)-2-[5-(4-Chloro-phenylcarbamoyl)-thiophene-3-sulfonylamino]-4-methyl-pentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 61-90-5,21675-61-6,25248-98-0,70-45-1
L-leucine

: 5-(4-chloro-phenylcarbamoyl)-thiophene-3-sulfonyl chloride

: 208775-93-3
(S)-2-[5-(4-Chloro-phenylcarbamoyl)-thiophene-3-sulfonylamino]-4-methyl-pentanoic acid

Guidance literature:: With triethylamine; In tetrahydrofuran; water; at 20 ℃; for 2h;
DOI:10.1007/BF02251685

Reference yield: 59.0%

: 67-56-1
methanol

: 208775-93-3
(S)-2-[5-(4-Chloro-phenylcarbamoyl)-thiophene-3-sulfonylamino]-4-methyl-pentanoic acid

: 208775-97-7
(S)-2-[5-(4-Chloro-phenylcarbamoyl)-thiophene-3-sulfonylamino]-4-methyl-pentanoic acid methyl ester

Guidance literature:: With thionyl chloride; for 4h; Ambient temperature;
DOI:10.1007/BF02251685

Reference yield: 52.0%

: 5680-79-5,883886-67-7
glycine ethyl ester hydrochloride

: 208775-93-3
(S)-2-[5-(4-Chloro-phenylcarbamoyl)-thiophene-3-sulfonylamino]-4-methyl-pentanoic acid

: {(S)-2-[5-(4-Chloro-phenylcarbamoyl)-thiophene-3-sulfonylamino]-4-methyl-pentanoylamino}-acetic acid methyl ester

Guidance literature:: With triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1.) 0 deg C, 2 h, 2.) room temperature, 2 h;
DOI:10.1007/BF02251685