P--P-methyldibenzophospholium frifluoromethanesulfonate

Base Information

• Chemical Name: P--P-methyldibenzophospholium frifluoromethanesulfonate
• CAS No.: 121192-34-5
• Molecular Formula: CF₃O₃S*C₂₇H₃₀OP
• Molecular Weight: 550.579
• Mol file: 121192-34-5.mol

Synonyms:P--P-methyldibenzophospholium frifluoromethanesulfonate

Chemical Property of P--P-methyldibenzophospholium frifluoromethanesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of P--P-methyldibenzophospholium frifluoromethanesulfonate

There total 2 articles about P--P-methyldibenzophospholium frifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-(2-cyclohexylvinyl)benzene (18869-27-7) → P--P-methyldibenzophospholium frifluoromethanesulfonate (121192-34-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 92 percent / MCPBA / CH₂Cl₂ / 20 h

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

DOI:10.1021/ja00197a055

Reference yield:

trans-1-Cyclohexyl-2-phenyloxirane (116544-25-3) + methyl trifluoromethanesulfonate (333-27-7) + 5H-benzo[b]phosphindole (244-87-1) → P--P-methyldibenzophospholium frifluoromethanesulfonate (121192-34-5)

Guidance literature:

Yield given. Multistep reaction;

DOI:10.1021/ja00197a055

upstream raw materials:

trans-1-Cyclohexyl-2-phenyloxirane

methyl trifluoromethanesulfonate

5H-benzo[b]phosphindole

(E)-(2-cyclohexylvinyl)benzene