1-chloro-1-phenyltetramethylgermole

Base Information

Chemical Name:1-chloro-1-phenyltetramethylgermole
CAS No.:127932-66-5
Molecular Formula:C₁₄H₁₇ClGe
Molecular Weight:293.332
Hs Code.:

Synonyms:1-chloro-1-phenyltetramethylgermole

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Chemical Property of 1-chloro-1-phenyltetramethylgermole

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Technology Process of 1-chloro-1-phenyltetramethylgermole

There total 2 articles about 1-chloro-1-phenyltetramethylgermole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 84101-39-3
1,1-bis(cyclopentadienyl)-2,3,4,5-tetramethylzirconacyclopentadiene

: 1074-29-9
trichlorophenylgermane

: 127932-66-5
1-chloro-1-phenyltetramethylgermole

Guidance literature:: In tetrahydrofuran; addn. of the metallacyclus in THF to the Ge compd. in THF, stirring at room temp. and heating in a sealed tube to 50°C for 10-30 min; evapn. (vac.) and extn.;
DOI:10.1016/0022-328X(90)87053-G

Reference yield:

: 56-23-5
tetrachloromethane

: 127932-68-7
1-phenyl-2,3,4,5-tetramethylgermole

: 127932-66-5
1-chloro-1-phenyltetramethylgermole

: 67-66-3,8013-54-5
chloroform

Guidance literature:: heating of the germole in CCl4 in a sealed tube at 90°C for 12 h; evapn. (vac.); elem. anal.;
DOI:10.1016/0022-328X(90)87053-G