6-[(3-{[(Benzyloxy)carbonyl](methyl)amino}propyl)(methyl)carbam oyl]pyridine-3-carboxylic acid

Base Information

Chemical Name:6-[(3-{[(Benzyloxy)carbonyl](methyl)amino}propyl)(methyl)carbam oyl]pyridine-3-carboxylic acid
CAS No.:1246246-77-4
Molecular Formula:C₂₀H₂₃N₃O₅
Molecular Weight:385.42
Hs Code.:

Synonyms:6-[(3-{[(Benzyloxy)carbonyl](methyl)amino}propyl)(methyl)carbam oyl]pyridine-3-carboxylic acid

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Chemical Property of 6-[(3-{[(Benzyloxy)carbonyl](methyl)amino}propyl)(methyl)carbam oyl]pyridine-3-carboxylic acid

Chemical Property:

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Technology Process of 6-[(3-{[(Benzyloxy)carbonyl](methyl)amino}propyl)(methyl)carbam oyl]pyridine-3-carboxylic acid

There total 3 articles about 6-[(3-{[(Benzyloxy)carbonyl](methyl)amino}propyl)(methyl)carbam oyl]pyridine-3-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 1246246-77-4
6-[(3-{[(Benzyloxy)carbonyl](methyl)amino}propyl)(methyl)carbam oyl]pyridine-3-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; pivaloyl chloride / dichloromethane / 0.25 h / 20 °C / Cooling with ice

1.2: 20 °C / Cooling with ice

1.3: 2 h / 20 °C / Cooling with ice

2.1: sodium hydroxide; water / methanol / 10 h / 50 °C

2.2: pH 3

With water; pivaloyl chloride; triethylamine; sodium hydroxide; In methanol; dichloromethane;

Reference yield:

: 111-33-1
1,3-bis(methylamino)propane

: 1246246-77-4
6-[(3-{[(Benzyloxy)carbonyl](methyl)amino}propyl)(methyl)carbam oyl]pyridine-3-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; pivaloyl chloride / dichloromethane / 0.25 h / 20 °C / Cooling with ice

1.2: 20 °C / Cooling with ice

1.3: 2 h / 20 °C / Cooling with ice

2.1: sodium hydroxide; water / methanol / 10 h / 50 °C

2.2: pH 3

With water; pivaloyl chloride; triethylamine; sodium hydroxide; In methanol; dichloromethane;

Reference yield:

: 17874-79-2
pyridine-2,5-dicarboxylic acid 5-methyl ester

: 1246246-77-4
6-[(3-{[(Benzyloxy)carbonyl](methyl)amino}propyl)(methyl)carbam oyl]pyridine-3-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; pivaloyl chloride / dichloromethane / 0.25 h / 20 °C / Cooling with ice

1.2: 20 °C / Cooling with ice

1.3: 2 h / 20 °C / Cooling with ice

2.1: sodium hydroxide; water / methanol / 10 h / 50 °C

2.2: pH 3

With water; pivaloyl chloride; triethylamine; sodium hydroxide; In methanol; dichloromethane;