C₃₂H₂₅NO₃

Base Information

Chemical Name:C₃₂H₂₅NO₃
CAS No.:1373243-62-9
Molecular Formula:C₃₂H₂₅NO₃
Molecular Weight:471.555
Hs Code.:

C<sub>32</sub>H<sub>25</sub>NO<sub>3</sub>

Synonyms:C₃₂H₂₅NO₃

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Chemical Property of C₃₂H₂₅NO₃

Chemical Property:

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Technology Process of C₃₂H₂₅NO₃

There total 10 articles about C₃₂H₂₅NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 593-71-5
Chloroiodomethane

: 1373243-61-8
1-benzhydryl-3-(6-hydroxy-3H-spiro[benzofuran-2,1'-cyclopropan]-5-yl)indolin-2-one

: 1373243-62-9
C₃₂H₂₅NO₃

Guidance literature:: 1-benzhydryl-3-(6-hydroxy-3H-spiro[benzofuran-2,1'-cyclopropan]-5-yl)indolin-2-one; With caesium carbonate; In tetrahydrofuran; at 20 ℃; for 0.5h;

Chloroiodomethane; In tetrahydrofuran; at 20 ℃; for 15h;

Reference yield:

: 6272-26-0
6-hydroxybenzofuran-3-one

: 1373243-62-9
C₃₂H₂₅NO₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 2.75 h / 0 - 50 °C / Inert atmosphere

3.1: lithium aluminium tetrahydride; aluminum (III) chloride / diethyl ether / 3 h / 0 - 20 °C / Inert atmosphere

3.2: 0 °C

4.1: hydrogen / palladium 10% on activated carbon / ethyl acetate; methanol / 3 h / 20 °C

5.1: isopropylmagnesium chloride / tetrahydrofuran / 1 h / 0 °C

5.2: 15 h / 0 - 20 °C

6.1: trifluoroacetic acid; triethylsilane / dichloromethane / 3 h / 0 - 10 °C

6.2: 0 °C

7.1: caesium carbonate / tetrahydrofuran / 0.5 h / 20 °C

7.2: 15 h / 20 °C

With triethylsilane; aluminum (III) chloride; lithium aluminium tetrahydride; hydrogen; isopropylmagnesium chloride; sodium hydride; potassium carbonate; caesium carbonate; trifluoroacetic acid; palladium 10% on activated carbon; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 1373243-55-0
6-(benzyloxy)-3H-spiro[benzofuran-2,1'-cyclopropan]-3-one

: 1373243-62-9
C₃₂H₂₅NO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium aluminium tetrahydride; aluminum (III) chloride / diethyl ether / 3 h / 0 - 20 °C / Inert atmosphere

1.2: 0 °C

2.1: hydrogen / palladium 10% on activated carbon / ethyl acetate; methanol / 3 h / 20 °C

3.1: isopropylmagnesium chloride / tetrahydrofuran / 1 h / 0 °C

3.2: 15 h / 0 - 20 °C

4.1: trifluoroacetic acid; triethylsilane / dichloromethane / 3 h / 0 - 10 °C

4.2: 0 °C

5.1: caesium carbonate / tetrahydrofuran / 0.5 h / 20 °C

5.2: 15 h / 20 °C

With triethylsilane; aluminum (III) chloride; lithium aluminium tetrahydride; hydrogen; isopropylmagnesium chloride; caesium carbonate; trifluoroacetic acid; palladium 10% on activated carbon; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; ethyl acetate;