2-(1,1-dicyanopropen-2-yl)-6-(2-(4-(2-cyclohexyl)ethyl)benzenesulfonyloxyethyl)methylamino-naphthalene

Base Information

Chemical Name:2-(1,1-dicyanopropen-2-yl)-6-(2-(4-(2-cyclohexyl)ethyl)benzenesulfonyloxyethyl)methylamino-naphthalene
CAS No.:1262387-15-4
Molecular Formula:C₃₂H₃₅N₃O₃S
Molecular Weight:541.714
Hs Code.:

Synonyms:2-(1,1-dicyanopropen-2-yl)-6-(2-(4-(2-cyclohexyl)ethyl)benzenesulfonyloxyethyl)methylamino-naphthalene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(1,1-dicyanopropen-2-yl)-6-(2-(4-(2-cyclohexyl)ethyl)benzenesulfonyloxyethyl)methylamino-naphthalene

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2-(1,1-dicyanopropen-2-yl)-6-(2-(4-(2-cyclohexyl)ethyl)benzenesulfonyloxyethyl)methylamino-naphthalene

There total 5 articles about 2-(1,1-dicyanopropen-2-yl)-6-(2-(4-(2-cyclohexyl)ethyl)benzenesulfonyloxyethyl)methylamino-naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1262387-07-4
4-(2-cyclohexyl-ethyl)-benzenesulfonyl chloride

: 259739-01-0
2-(1-(6-((2-hydroxyethyl)(methyl)amino)naphthalen-2-yl)ethylidene)malononitrile

: 1262387-15-4
2-(1,1-dicyanopropen-2-yl)-6-(2-(4-(2-cyclohexyl)ethyl)benzenesulfonyloxyethyl)methylamino-naphthalene

Guidance literature:: With pyridine; at 20 ℃; for 4h;

Reference yield:

: 2043-61-0
cyclohexanecarbaldehyde

: 1262387-15-4
2-(1,1-dicyanopropen-2-yl)-6-(2-(4-(2-cyclohexyl)ethyl)benzenesulfonyloxyethyl)methylamino-naphthalene

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C

2.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 8 h / 20 °C

3.1: chlorosulfonic acid; sodium chloride / chloroform / 0 - 20 °C

4.1: pyridine / 4 h / 20 °C

With pyridine; chlorosulfonic acid; hydrogen; sodium chloride; lithium diisopropyl amide; palladium 10% on activated carbon; In tetrahydrofuran; chloroform; ethyl acetate;

Reference yield:

: 18869-27-7
(E)-(2-cyclohexylvinyl)benzene

: 1262387-15-4
2-(1,1-dicyanopropen-2-yl)-6-(2-(4-(2-cyclohexyl)ethyl)benzenesulfonyloxyethyl)methylamino-naphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 8 h / 20 °C

2: chlorosulfonic acid; sodium chloride / chloroform / 0 - 20 °C

3: pyridine / 4 h / 20 °C

With pyridine; chlorosulfonic acid; hydrogen; sodium chloride; palladium 10% on activated carbon; In chloroform; ethyl acetate;