Technology Process of C38H48N4OS
There total 13 articles about C38H48N4OS which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium cyanoborohydride;
acetic acid;
In
methanol;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogenchloride / 1,4-dioxane; iso-butanol / 1 h / 90 °C
2: hydrazine / ethanol / 16 h / 20 °C
3: sodium cyanoborohydride / acetic acid / methanol
With
hydrogenchloride; sodium cyanoborohydride; hydrazine;
acetic acid;
In
1,4-dioxane; methanol; ethanol; iso-butanol;
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: nitronium tetrafluoborate / 1,2-dimethoxyethane / 4 h / -55 - -10 °C
2.1: hydrogen / palladium 10% on activated carbon / ethanol; ethyl acetate / 5 h / 1140.08 Torr
3.1: tetrahydrofuran / 16 h / Heating / reflux
4.1: sodium hydroxide; water / ethanol / 1.5 h / Heating / reflux
5.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.17 h
5.2: 20 °C
6.1: sodium hydride / N,N-dimethyl-formamide / 1.5 h
6.2: 5 - 20 °C
7.1: hydrogenchloride / 1,4-dioxane; iso-butanol / 1 h / 90 °C
8.1: hydrazine / ethanol / 16 h / 20 °C
9.1: sodium cyanoborohydride / acetic acid / methanol
With
hydrogenchloride; dmap; sodium hydroxide; nitronium tetrafluoborate; water; hydrogen; sodium hydride; sodium cyanoborohydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydrazine;
palladium 10% on activated carbon; acetic acid;
In
tetrahydrofuran; 1,4-dioxane; methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; iso-butanol;
