5-(2,5-dimethoxy-4-(dimethoxymethyl)phenyl)-13,17-dibutyl-2,3,7,8,12,18-hexamethylporphine

Base Information

Chemical Name:5-(2,5-dimethoxy-4-(dimethoxymethyl)phenyl)-13,17-dibutyl-2,3,7,8,12,18-hexamethylporphine
CAS No.:133677-84-6
Molecular Formula:C₄₅H₅₆N₄O₄
Molecular Weight:716.964
Hs Code.:

Synonyms:5-(2,5-dimethoxy-4-(dimethoxymethyl)phenyl)-13,17-dibutyl-2,3,7,8,12,18-hexamethylporphine

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Chemical Property of 5-(2,5-dimethoxy-4-(dimethoxymethyl)phenyl)-13,17-dibutyl-2,3,7,8,12,18-hexamethylporphine

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Technology Process of 5-(2,5-dimethoxy-4-(dimethoxymethyl)phenyl)-13,17-dibutyl-2,3,7,8,12,18-hexamethylporphine

There total 1 articles about 5-(2,5-dimethoxy-4-(dimethoxymethyl)phenyl)-13,17-dibutyl-2,3,7,8,12,18-hexamethylporphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 67-56-1
methanol

: 127665-37-6
8,12-dibutyl-2,3,7,13,17,18-hexamethylbiladiene-ac-21,24-diium dibromide

: 7310-97-6
2,5-dimethoxyterephthalaldehyde

: 133677-84-6
5-(2,5-dimethoxy-4-(dimethoxymethyl)phenyl)-13,17-dibutyl-2,3,7,8,12,18-hexamethylporphine

Guidance literature:: With hydrogen bromide; acetic acid; for 41h; Heating;
DOI:10.1246/bcsj.64.29

Reference yield: 99.0%

: 133677-84-6
5-(2,5-dimethoxy-4-(dimethoxymethyl)phenyl)-13,17-dibutyl-2,3,7,8,12,18-hexamethylporphine

: 133895-51-9
5-(2,5-hydroxy-4-formylphenyl)-13,17-dibutyl-2,3,7,8,12,18-hexamethylporphine

Guidance literature:: With boron tribromide; In dichloromethane;
DOI:10.1246/bcsj.64.29

Reference yield:

: 133677-84-6
5-(2,5-dimethoxy-4-(dimethoxymethyl)phenyl)-13,17-dibutyl-2,3,7,8,12,18-hexamethylporphine

: 133677-85-7
5-(2-acetoxy-4-formyl-5-hydroxyphenyl)-13,17-dibutyl-2,3,7,8,12,18-hexamethylporphine

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / BBr₃ / CH₂Cl₂

2: 32 percent / pyridine / CH₂Cl₂ / 48 h

With pyridine; boron tribromide; In dichloromethane;
DOI:10.1246/bcsj.64.29