C₅₁H₅₆O₁₀

Base Information

Chemical Name:C₅₁H₅₆O₁₀
CAS No.:1422178-94-6
Molecular Formula:C₅₁H₅₆O₁₀
Molecular Weight:829
Hs Code.:

C<sub>51</sub>H<sub>56</sub>O<sub>10</sub>

Synonyms:C₅₁H₅₆O₁₀

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Chemical Property of C₅₁H₅₆O₁₀

Chemical Property:

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Technology Process of C₅₁H₅₆O₁₀

There total 6 articles about C₅₁H₅₆O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: C₅₀H₅₂O₉

: 1422178-86-6
C₅₁H₅₆O₁₀

: 1422178-94-6
C₅₁H₅₆O₁₀

Guidance literature:: With palladium diacetate; at 20 ℃; for 2.5h; Inert atmosphere;
DOI:10.1016/j.tet.2012.12.065

Reference yield:

: 37776-17-3
5,6-anhydro-3-O-benzyl-1,2-O-isopropylidene-β-L-idofuranose

: 1422178-94-6
C₅₁H₅₆O₁₀

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C / Inert atmosphere

1.2: 0.33 h / -78 °C / Inert atmosphere

1.3: 2 h / -78 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 6 h / 0 - 20 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

4.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / Reflux

5.1: palladium diacetate / 2.5 h / 20 °C / Inert atmosphere

With n-butyllithium; tetrabutyl ammonium fluoride; palladium diacetate; sodium hydride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; hexane; ethyl acetate; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.tet.2012.12.065

Reference yield:

: 1319725-94-4
tert-butyldimethyl((2R,3S,4S)-1,3,4-tris(benzyloxy)hex-5-yn-2-yloxy)silane

: 1422178-94-6
C₅₁H₅₆O₁₀

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C / Inert atmosphere

1.2: 0.33 h / -78 °C / Inert atmosphere

1.3: 2 h / -78 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 6 h / 0 - 20 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

4.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / Reflux

5.1: palladium diacetate / 2.5 h / 20 °C / Inert atmosphere

With n-butyllithium; tetrabutyl ammonium fluoride; palladium diacetate; sodium hydride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; hexane; ethyl acetate; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.tet.2012.12.065