Technology Process of C25H30N4O3S
There total 12 articles about C25H30N4O3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium azide;
In
water; acetone;
Yield given;
Ambient temperature;
DOI:10.1021/jo00107a009
- Guidance literature:
-
Multi-step reaction with 10 steps
1: 100 percent / acetonitrile / 16 h / Heating
2: 78 percent / LDA / tetrahydrofuran; hexane / 1.) room temp., 30 min, 2.) room temp, 1 h
3: 95 percent / Na, NH3(l) / 2 h
4: diethyl ether
5: NaH / tetrahydrofuran / 0 °C
6: HCl / diethyl ether / 0 °C
8: NaCNBH3 / tetrahydrofuran; H2O / 3 h / Ambient temperature; pH 4
9: DBU / CH2Cl2 / -78 °C
10: NaN3 / acetone; H2O / Ambient temperature
With
hydrogenchloride; sodium azide; ammonia; sodium; sodium hydride; sodium cyanoborohydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium diisopropyl amide;
In
tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; acetone; acetonitrile;
DOI:10.1021/jo00107a009
- Guidance literature:
-
Multi-step reaction with 6 steps
1: NaH / tetrahydrofuran / 0 °C
2: HCl / diethyl ether / 0 °C
4: NaCNBH3 / tetrahydrofuran; H2O / 3 h / Ambient temperature; pH 4
5: DBU / CH2Cl2 / -78 °C
6: NaN3 / acetone; H2O / Ambient temperature
With
hydrogenchloride; sodium azide; sodium hydride; sodium cyanoborohydride; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
tetrahydrofuran; diethyl ether; dichloromethane; water; acetone;
DOI:10.1021/jo00107a009
