3,5-Di-tert-butyl-5-(3,5-di-tert-butyl-2-hydroxy-phenylazo)-5H-furan-2-one

Base Information

• Chemical Name: 3,5-Di-tert-butyl-5-(3,5-di-tert-butyl-2-hydroxy-phenylazo)-5H-furan-2-one
• CAS No.: 78749-34-5
• Molecular Formula: C₂₆H₄₀N₂O₃
• Molecular Weight: 428.615

Synonyms:3,5-Di-tert-butyl-5-(3,5-di-tert-butyl-2-hydroxy-phenylazo)-5H-furan-2-one

Chemical Property of 3,5-Di-tert-butyl-5-(3,5-di-tert-butyl-2-hydroxy-phenylazo)-5H-furan-2-one

Chemical Property:

Purity/Quality:

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Technology Process of 3,5-Di-tert-butyl-5-(3,5-di-tert-butyl-2-hydroxy-phenylazo)-5H-furan-2-one

There total 3 articles about 3,5-Di-tert-butyl-5-(3,5-di-tert-butyl-2-hydroxy-phenylazo)-5H-furan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

2,4-di-tert-butyl-6-diazo-2,4-cyclohexadienone (856632-67-2,78448-34-7) → 3,5-Di-tert-butyl-5-(3,5-di-tert-butyl-2-hydroxy-phenylazo)-5H-furan-2-one (78749-34-5) + 1,6-Di-tert-butyl-4-methoxy-2,3-dioxa-bicyclo[3.2.1]oct-6-en-8-one (82959-56-6)

Guidance literature:

With oxygen; methylene blue; In methanol; for 12h; Irradiation;

DOI:10.1021/ja00406a051

Reference yield: 60.0%

methanol (67-56-1) + 2,4-di-tert-butyl-6-diazo-2,4-cyclohexadienone (856632-67-2,78448-34-7) → 3,5-Di-tert-butyl-5-(3,5-di-tert-butyl-2-hydroxy-phenylazo)-5H-furan-2-one (78749-34-5) + 1,6-Di-tert-butyl-4-methoxy-2,3-dioxa-bicyclo[3.2.1]oct-6-en-8-one (82959-56-6)

Guidance literature:

With oxygen; methylene blue; for 12h; Product distribution; Irradiation; other solvent, sensitizer; photosensitized oxygenation of α-diazoquinone;

DOI:10.1021/ja00406a051

Reference yield: 13.0%

2,4-di-tert-butyl-6-diazo-2,4-cyclohexadienone (856632-67-2,78448-34-7) → 3,5-Di-tert-butyl-5-(3,5-di-tert-butyl-2-hydroxy-phenylazo)-5H-furan-2-one (78749-34-5) + α,γ-di-tert-butyl-γ-crotonolactone (53904-87-3)

Guidance literature:

With oxygen; thiamine diphosphate; In benzene; at 25 ℃; Irradiation;

DOI:10.1021/ja00406a051

upstream raw materials:

methanol

2,4-di-tert-butyl-6-diazo-2,4-cyclohexadienone

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