7-ethoxy-4-(4-fluoro-3-trifluoromethylanilino)-6-methoxy-1,2,3-benzotriazine

Base Information

Chemical Name:7-ethoxy-4-(4-fluoro-3-trifluoromethylanilino)-6-methoxy-1,2,3-benzotriazine
CAS No.:1048698-73-2
Molecular Formula:C₁₇H₁₄F₄N₄O₂
Molecular Weight:382.317
Hs Code.:

Synonyms:7-ethoxy-4-(4-fluoro-3-trifluoromethylanilino)-6-methoxy-1,2,3-benzotriazine

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Chemical Property of 7-ethoxy-4-(4-fluoro-3-trifluoromethylanilino)-6-methoxy-1,2,3-benzotriazine

Chemical Property:

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Technology Process of 7-ethoxy-4-(4-fluoro-3-trifluoromethylanilino)-6-methoxy-1,2,3-benzotriazine

There total 6 articles about 7-ethoxy-4-(4-fluoro-3-trifluoromethylanilino)-6-methoxy-1,2,3-benzotriazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₇H₁₄F₄N₄O₂

: 1048698-73-2
7-ethoxy-4-(4-fluoro-3-trifluoromethylanilino)-6-methoxy-1,2,3-benzotriazine

Guidance literature:: C₁₇H₁₄F₄N₄O₂; In ethanol; for 1h; Reflux;

With acetic acid; In ethanol; for 2h; Reflux;
DOI:10.1016/j.bmc.2013.10.009

Reference yield:

: 4421-08-3
3-methoxy-4-hydroxybenzonitrile

: 1048698-73-2
7-ethoxy-4-(4-fluoro-3-trifluoromethylanilino)-6-methoxy-1,2,3-benzotriazine

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

1.2: 20 - 37 °C

2.1: nitric acid / 2 h / 30 °C

3.1: cyclohexene; palladium 10% on activated carbon / ethanol / Reflux

4.1: hydrogenchloride; sodium nitrite / water / 0 °C

4.2: 2 h / 0 °C

5.1: ethanol / 1 h / Reflux

5.2: 2 h / Reflux

With hydrogenchloride; palladium 10% on activated carbon; nitric acid; potassium carbonate; cyclohexene; sodium nitrite; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2013.10.009

Reference yield:

: 81259-56-5
4-ethoxy-3-methoxybenzonitrile

: 1048698-73-2
7-ethoxy-4-(4-fluoro-3-trifluoromethylanilino)-6-methoxy-1,2,3-benzotriazine

Guidance literature:: Multi-step reaction with 4 steps

1.1: nitric acid / 2 h / 30 °C

2.1: cyclohexene; palladium 10% on activated carbon / ethanol / Reflux

3.1: hydrogenchloride; sodium nitrite / water / 0 °C

3.2: 2 h / 0 °C

4.1: ethanol / 1 h / Reflux

4.2: 2 h / Reflux

With hydrogenchloride; palladium 10% on activated carbon; nitric acid; cyclohexene; sodium nitrite; In ethanol; water;
DOI:10.1016/j.bmc.2013.10.009