4-nitrophenylacetyl fluoride

Base Information

Chemical Name:4-nitrophenylacetyl fluoride
CAS No.:78507-53-6
Molecular Formula:C₈H₆FNO₃
Molecular Weight:183.139
Hs Code.:

Synonyms:4-nitrophenylacetyl fluoride

Suppliers and Price of 4-nitrophenylacetyl fluoride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-nitrophenylacetyl fluoride

Chemical Property:

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Technology Process of 4-nitrophenylacetyl fluoride

There total 1 articles about 4-nitrophenylacetyl fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 104-03-0
4-nitrobenzeneacetic acid

: 78507-53-6
4-nitrophenylacetyl fluoride

Guidance literature:: With pyridine; trifluoro-[1,3,5]triazine; In acetonitrile; at 20 ℃; for 3.5h;
DOI:10.1002/jlcr.899

Reference yield: 34.0%

: 40217-17-2,90719-32-7,120574-96-1,102029-44-7
(R)-4-(phenylmethyl)-2-oxazolidinone

: 78507-53-6
4-nitrophenylacetyl fluoride

: 869304-72-3
4R-benzyl-3-(4-nitrophenylacetyl)-2-oxazolidinone

Guidance literature:: With n-butyllithium; triphenylmethane; In tetrahydrofuran; hexane; at -78 ℃; for 1h;
DOI:10.1002/jlcr.899

Reference yield:

: 78507-53-6
4-nitrophenylacetyl fluoride

: 376594-64-8
R-2-(4-aminophenyl)-1-(2-propanesulfonamido)-propane

Guidance literature:: Multi-step reaction with 7 steps

1: 34 percent / triphenylmethane; n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

2: 33 percent / sodium bis(trimethylsilyl)amide / tetrahydrofuran; toluene / -70 - 20 °C

3: 91 percent / sodium borohydride / tetrahydrofuran; H₂O / 3 h / 20 °C

4: 88 percent / triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 18 h / 20 °C

5: 95 percent / hydrazine / toluene / 1 h / 80 - 90 °C

6: 88 percent / triethylamine; 4-(dimethylamino)pyridine / CH₂Cl₂ / 18 h / 20 °C

7: 88 percent / hydrogen / Pd/C / ethanol / 16 h

With dmap; sodium tetrahydroborate; n-butyllithium; triphenylmethane; hydrogen; sodium hexamethyldisilazane; triethylamine; triphenylphosphine; hydrazine; diethylazodicarboxylate; palladium on activated charcoal; In tetrahydrofuran; ethanol; hexane; dichloromethane; water; toluene; 4: Mitsunobu reaction;
DOI:10.1002/jlcr.899