(E)-5-(2-carbomethoxyvinyl)-1-(2'-deoxy-3',5'-di-O-p-toluoyl-β-D-erythro-pentafuranosyl)-6-azauracil

Base Information

Chemical Name:(E)-5-(2-carbomethoxyvinyl)-1-(2'-deoxy-3',5'-di-O-p-toluoyl-β-D-erythro-pentafuranosyl)-6-azauracil
CAS No.:97776-67-5
Molecular Formula:C₂₈H₂₇N₃O₉
Molecular Weight:549.537
Hs Code.:

Synonyms:(E)-5-(2-carbomethoxyvinyl)-1-(2'-deoxy-3',5'-di-O-p-toluoyl-β-D-erythro-pentafuranosyl)-6-azauracil

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Chemical Property of (E)-5-(2-carbomethoxyvinyl)-1-(2'-deoxy-3',5'-di-O-p-toluoyl-β-D-erythro-pentafuranosyl)-6-azauracil

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Technology Process of (E)-5-(2-carbomethoxyvinyl)-1-(2'-deoxy-3',5'-di-O-p-toluoyl-β-D-erythro-pentafuranosyl)-6-azauracil

There total 2 articles about (E)-5-(2-carbomethoxyvinyl)-1-(2'-deoxy-3',5'-di-O-p-toluoyl-β-D-erythro-pentafuranosyl)-6-azauracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 97776-66-4
5-formyl-1-(2'-deoxy-3'-5'-di-O-p-toluoyl-β-D-erythro-pentofuranosyl)-6-azauracil

: 21204-67-1,2605-67-6
methyl (triphenylphosphoranylidene)acetate

: 97776-67-5
(E)-5-(2-carbomethoxyvinyl)-1-(2'-deoxy-3',5'-di-O-p-toluoyl-β-D-erythro-pentafuranosyl)-6-azauracil

Guidance literature:: In acetonitrile; for 5h; Heating;
DOI:10.1021/jm00155a035

Reference yield:

: 20258-32-6
5-hydroxymethyl-(3,5-di-O-p-toluoyl)-6-aza-2-deoxyuridine

: 97776-67-5
(E)-5-(2-carbomethoxyvinyl)-1-(2'-deoxy-3',5'-di-O-p-toluoyl-β-D-erythro-pentafuranosyl)-6-azauracil

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / diphenyl diselenide, 70percent aq. tert-butyl hydroperoxide / benzene / 4.5 h / Heating

2: 85 percent / acetonitrile / 5 h / Heating

With tert.-butylhydroperoxide; diphenyl diselenide; In acetonitrile; benzene;
DOI:10.1021/jm00155a035