dimethyl ((3-chlorophenyl)((4-methylphenyl)sulfonamido)methyl)phosphonate

Base Information

Chemical Name:dimethyl ((3-chlorophenyl)((4-methylphenyl)sulfonamido)methyl)phosphonate
CAS No.:1154063-20-3
Molecular Formula:C₁₆H₁₉ClNO₅PS
Molecular Weight:403.823
Hs Code.:

Synonyms:dimethyl ((3-chlorophenyl)((4-methylphenyl)sulfonamido)methyl)phosphonate

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Chemical Property of dimethyl ((3-chlorophenyl)((4-methylphenyl)sulfonamido)methyl)phosphonate

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Technology Process of dimethyl ((3-chlorophenyl)((4-methylphenyl)sulfonamido)methyl)phosphonate

There total 4 articles about dimethyl ((3-chlorophenyl)((4-methylphenyl)sulfonamido)methyl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 36198-87-5
dimethyl trimethylsilyl phosphite

: 169829-11-2
N-(m-chlorobenzylidene)-4-methylbenzenesulfonamide

: 1154063-20-3
dimethyl ((3-chlorophenyl)((4-methylphenyl)sulfonamido)methyl)phosphonate

Guidance literature:: With iodine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jo9003162

Reference yield: 84.0%

: 96-36-6,868-85-9
methyl phosphite

: 169829-11-2
N-(m-chlorobenzylidene)-4-methylbenzenesulfonamide

: 1154063-20-3
dimethyl ((3-chlorophenyl)((4-methylphenyl)sulfonamido)methyl)phosphonate

Guidance literature:: With triethylamine; In toluene; for 24h; Reflux; Inert atmosphere;
DOI:10.1021/acs.orglett.9b03669

Reference yield:

: 70-55-3
toluene-4-sulfonamide

: 1154063-20-3
dimethyl ((3-chlorophenyl)((4-methylphenyl)sulfonamido)methyl)phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / toluene / Reflux; Inert atmosphere; Dean-Stark

2: triethylamine / toluene / 24 h / Reflux; Inert atmosphere

With boron trifluoride diethyl etherate; triethylamine; In toluene;
DOI:10.1021/acs.orglett.9b03669