(E)-(-)-(1'R,2'R)-N-methyl-N-(2'-phenyl-2'-hydroxy-1'-methylethyl)but-2-enamide

Base Information

Chemical Name:(E)-(-)-(1'R,2'R)-N-methyl-N-(2'-phenyl-2'-hydroxy-1'-methylethyl)but-2-enamide
CAS No.:1061728-06-0
Molecular Formula:C₁₄H₁₉NO₂
Molecular Weight:233.31
Hs Code.:

Synonyms:(E)-(-)-(1'R,2'R)-N-methyl-N-(2'-phenyl-2'-hydroxy-1'-methylethyl)but-2-enamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-(-)-(1'R,2'R)-N-methyl-N-(2'-phenyl-2'-hydroxy-1'-methylethyl)but-2-enamide

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Technology Process of (E)-(-)-(1'R,2'R)-N-methyl-N-(2'-phenyl-2'-hydroxy-1'-methylethyl)but-2-enamide

There total 1 articles about (E)-(-)-(1'R,2'R)-N-methyl-N-(2'-phenyl-2'-hydroxy-1'-methylethyl)but-2-enamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 625-35-4,3488-22-0,10487-71-5
trans-chrotonyl chloride

: 321-97-1,7009-81-6,90-83-5,6912-63-6
(1R,2R)-pseudoephedrine

: 1061728-06-0
(E)-(-)-(1'R,2'R)-N-methyl-N-(2'-phenyl-2'-hydroxy-1'-methylethyl)but-2-enamide

Guidance literature:: With triethylamine; In tetrahydrofuran; at -20 ℃; for 1.5h;
DOI:10.1016/j.tetasy.2008.06.017

Reference yield: 93.0%

: 1061728-06-0
(E)-(-)-(1'R,2'R)-N-methyl-N-(2'-phenyl-2'-hydroxy-1'-methylethyl)but-2-enamide

: 693-25-4
n-pentylmagnesium bromide

: (-)-(1'R,2'R)-N-methyl-N-(2'-phenyl-2'-hydroxy-1'-methylethyl)-3-methyloctanamide

Guidance literature:: With copper(I) bromide dimethylsulfide complex; In diethyl ether; dichloromethane; at -30 ℃; for 6h;
DOI:10.1016/j.tetasy.2008.06.017

Reference yield: 92.0%

: 1061728-06-0
(E)-(-)-(1'R,2'R)-N-methyl-N-(2'-phenyl-2'-hydroxy-1'-methylethyl)but-2-enamide

: 1730-25-2
allylmagnesium bromide

: (-)-(1'R,2'R)-N-methyl-N-(2'-phenyl-2'-hydroxy-1'-methylethyl)-3-methylhex-5-enamide

Guidance literature:: With copper(I) bromide dimethylsulfide complex; In diethyl ether; dichloromethane; at -30 ℃; for 6h;
DOI:10.1016/j.tetasy.2008.06.017