Methyl (2S)-2-[(mesitylsulfonyl)amino]-3-(3'-{[(Z)-1-(methyl-sulfanyl)-2-nitroethenyl]amino}[1,1'-biphenyl]-4-yl)-propanoate

Base Information

• Chemical Name: Methyl (2S)-2-[(mesitylsulfonyl)amino]-3-(3'-{[(Z)-1-(methyl-sulfanyl)-2-nitroethenyl]amino}[1,1'-biphenyl]-4-yl)-propanoate
• CAS No.: 276258-91-4
• Molecular Formula: C₂₈H₃₁N₃O₆S₂
• Molecular Weight: 569.703

Synonyms:Methyl (2S)-2-[(mesitylsulfonyl)amino]-3-(3'-{[(Z)-1-(methyl-sulfanyl)-2-nitroethenyl]amino}[1,1'-biphenyl]-4-yl)-propanoate

Chemical Property of Methyl (2S)-2-[(mesitylsulfonyl)amino]-3-(3'-{[(Z)-1-(methyl-sulfanyl)-2-nitroethenyl]amino}[1,1'-biphenyl]-4-yl)-propanoate

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Technology Process of Methyl (2S)-2-[(mesitylsulfonyl)amino]-3-(3'-{[(Z)-1-(methyl-sulfanyl)-2-nitroethenyl]amino}[1,1'-biphenyl]-4-yl)-propanoate

There total 2 articles about Methyl (2S)-2-[(mesitylsulfonyl)amino]-3-(3'-{[(Z)-1-(methyl-sulfanyl)-2-nitroethenyl]amino}[1,1'-biphenyl]-4-yl)-propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

methyl (2S)-3-(3'-amino[1,1'-biphenyl]-4-yl)-2-mesitylsulfonylamino-propanoate (276258-90-3) + 1,1-di(methylsulfanyl)-2-nitroethylene (13623-94-4) → Methyl (2S)-2-[(mesitylsulfonyl)amino]-3-(3'-{[(Z)-1-(methyl-sulfanyl)-2-nitroethenyl]amino}[1,1'-biphenyl]-4-yl)-propanoate (276258-91-4)

Guidance literature:

In propan-1-ol; for 4h; Heating / reflux;

Reference yield:

1,1-bis(thiomethyl)-2-nitroethylene + methyl (2S)-3-(3-amino[1,1'-biphenyl]-4-yl)-2-mesitylsulfonylamino-propanoate → Methyl (2S)-2-[(mesitylsulfonyl)amino]-3-(3'-{[(Z)-1-(methyl-sulfanyl)-2-nitroethenyl]amino}[1,1'-biphenyl]-4-yl)-propanoate (276258-91-4)

Guidance literature:

In propan-1-ol;

Reference yield: 86.0%

Methyl (2S)-2-[(mesitylsulfonyl)amino]-3-(3'-{[(Z)-1-(methyl-sulfanyl)-2-nitroethenyl]amino}[1,1'-biphenyl]-4-yl)-propanoate (276258-91-4) + Cyclopropylamine (765-30-0) → methyl (2S)-3-(3'-{[(E)-1-(cyclopropylamino)-2-nitroethenyl]-amino}[1,1'-biphenyl]-4-yl)-2-[(mesitylsulfonyl)amino]-propanoate (276258-92-5)

Guidance literature:

In propan-1-ol; for 1h; Heating / reflux;

upstream raw materials:

methyl (2S)-3-(3'-amino[1,1'-biphenyl]-4-yl)-2-mesitylsulfonylamino-propanoate

1,1-di(methylsulfanyl)-2-nitroethylene

Downstream raw materials:

methyl (2S)-3-(3'-{[(E)-1-(cyclopropylamino)-2-nitroethenyl]-amino}[1,1'-biphenyl]-4-yl)-2-[(mesitylsulfonyl)amino]-propanoate

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