1-[4-(2-methacryloyloxyethyl)aminocarbonyloxymethylphenyl]-3-methyl-3-[(2-methacryloyloxyethyl)amino-(2-carbonyloxyethyl)]triaz-1-ene

Base Information

Chemical Name:1-[4-(2-methacryloyloxyethyl)aminocarbonyloxymethylphenyl]-3-methyl-3-[(2-methacryloyloxyethyl)amino-(2-carbonyloxyethyl)]triaz-1-ene
CAS No.:609852-69-9
Molecular Formula:C₂₄H₃₃N₅O₈
Molecular Weight:519.555
Hs Code.:

Synonyms:1-[4-(2-methacryloyloxyethyl)aminocarbonyloxymethylphenyl]-3-methyl-3-[(2-methacryloyloxyethyl)amino-(2-carbonyloxyethyl)]triaz-1-ene

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Chemical Property of 1-[4-(2-methacryloyloxyethyl)aminocarbonyloxymethylphenyl]-3-methyl-3-[(2-methacryloyloxyethyl)amino-(2-carbonyloxyethyl)]triaz-1-ene

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Technology Process of 1-[4-(2-methacryloyloxyethyl)aminocarbonyloxymethylphenyl]-3-methyl-3-[(2-methacryloyloxyethyl)amino-(2-carbonyloxyethyl)]triaz-1-ene

There total 4 articles about 1-[4-(2-methacryloyloxyethyl)aminocarbonyloxymethylphenyl]-3-methyl-3-[(2-methacryloyloxyethyl)amino-(2-carbonyloxyethyl)]triaz-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 30674-80-7
2-Isocyanatoethyl methacrylate

: 197249-59-5
1-(4-hydroxymethylphenyl)-3-methyl-3-(2-hydroxyethyl)triaz-1-ene

: 609852-69-9
1-[4-(2-methacryloyloxyethyl)aminocarbonyloxymethylphenyl]-3-methyl-3-[(2-methacryloyloxyethyl)amino-(2-carbonyloxyethyl)]triaz-1-ene

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; dibutyltin dilaurate; 4-methoxy-phenol; In tetrahydrofuran; for 24h; Inert atmosphere; Reflux;
DOI:10.1016/j.reactfunctpolym.2012.04.014

Reference yield:

: 94-09-7
p-aminoethylbenzoate

: 609852-69-9
1-[4-(2-methacryloyloxyethyl)aminocarbonyloxymethylphenyl]-3-methyl-3-[(2-methacryloyloxyethyl)amino-(2-carbonyloxyethyl)]triaz-1-ene

Guidance literature:: Multi-step reaction with 4 steps

1: tert.-butylnitrite; boron trifluoride diethyl etherate / tetrahydrofuran; dichloromethane / -25 - -20 °C

2: sodium carbonate / tetrahydrofuran; water / 15 h / 0 - 20 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 6 h / 50 °C / Inert atmosphere

4: 1,4-diaza-bicyclo[2.2.2]octane; dibutyltin dilaurate; 4-methoxy-phenol / tetrahydrofuran / 24 h / Inert atmosphere; Reflux

With 1,4-diaza-bicyclo[2.2.2]octane; lithium aluminium tetrahydride; tert.-butylnitrite; boron trifluoride diethyl etherate; sodium carbonate; dibutyltin dilaurate; 4-methoxy-phenol; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.reactfunctpolym.2012.04.014

Reference yield:

: 348-06-1
p-carboethoxybenzenediazonium tetrafluoroborate

: 609852-69-9
1-[4-(2-methacryloyloxyethyl)aminocarbonyloxymethylphenyl]-3-methyl-3-[(2-methacryloyloxyethyl)amino-(2-carbonyloxyethyl)]triaz-1-ene

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate / tetrahydrofuran; water / 15 h / 0 - 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 6 h / 50 °C / Inert atmosphere

3: 1,4-diaza-bicyclo[2.2.2]octane; dibutyltin dilaurate; 4-methoxy-phenol / tetrahydrofuran / 24 h / Inert atmosphere; Reflux

With 1,4-diaza-bicyclo[2.2.2]octane; lithium aluminium tetrahydride; sodium carbonate; dibutyltin dilaurate; 4-methoxy-phenol; In tetrahydrofuran; water;
DOI:10.1016/j.reactfunctpolym.2012.04.014