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30674-80-7

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  • 2-Isocyanatoethyl methacrylate CAS 30674-80-7 MOI IN STOCK Methacryloyloxyethyl isocyanate CAS 30674-80-7

    Cas No: 30674-80-7

  • USD $ 3.5-5.0 / Kiloliter

  • 5 Kiloliter

  • 3000 Metric Ton/Month

  • Chemwill Asia Co., Ltd.
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30674-80-7 Usage

Chemical Properties

Colorless liquid

Uses

Different sources of media describe the Uses of 30674-80-7 differently. You can refer to the following data:
1. A latent cross-linker for resins.
2. A latent cross-linker for resins.1

General Description

Liquid.

Reactivity Profile

Isocyanates and thioisocyanates, such as 2-Isocyanatoethyl methacrylate, are incompatible with many classes of compounds, reacting exothermically to release toxic gases. Reactions with amines, aldehydes, alcohols, alkali metals, ketones, mercaptans, strong oxidizers, hydrides, phenols, and peroxides can cause vigorous releases of heat. Acids and bases initiate polymerization reactions in these materials. Some isocyanates react with water to form amines and liberate carbon dioxide.

Health Hazard

(Non-Specific -- Isocyanates and Solutions, n.o.s. (Flammable, Poisonous)) Poisonous; may be fatal if inhaled, swallowed or absorbed through skin. Contact may cause burns to skin and eyes.

Fire Hazard

(Non-Specific -- Isocyanates and Solutions, n.o.s. (Flammable, Poisonous)) May be ignited by heat, sparks, or flames. Container may explode in heat of fire. Vapor explosion and poison hazard indoors, outdoors or in sewers. Runoff from fire control or dilution water may cause pollution.

Flammability and Explosibility

Notclassified

Check Digit Verification of cas no

The CAS Registry Mumber 30674-80-7 includes 8 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 5 digits, 3,0,6,7 and 4 respectively; the second part has 2 digits, 8 and 0 respectively.
Calculate Digit Verification of CAS Registry Number 30674-80:
(7*3)+(6*0)+(5*6)+(4*7)+(3*4)+(2*8)+(1*0)=107
107 % 10 = 7
So 30674-80-7 is a valid CAS Registry Number.
InChI:InChI=1/C7H9NO3/c1-5(2)7(10)11-6(3)8-4-9/h6H,1H2,2-3H3

30674-80-7 Well-known Company Product Price

  • Brand
  • (Code)Product description
  • CAS number
  • Packaging
  • Price
  • Detail
  • Aldrich

  • (477060)  2-Isocyanatoethylmethacrylate  contains ≤0.1% BHT as inhibitor, 98%

  • 30674-80-7

  • 477060-5ML

  • 1,319.76CNY

  • Detail
  • Aldrich

  • (477060)  2-Isocyanatoethylmethacrylate  contains ≤0.1% BHT as inhibitor, 98%

  • 30674-80-7

  • 477060-50ML

  • 6,598.80CNY

  • Detail

30674-80-7SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 13, 2017

Revision Date: Aug 13, 2017

1.Identification

1.1 GHS Product identifier

Product name 2-isocyanatoethyl 2-methylprop-2-enoate

1.2 Other means of identification

Product number -
Other names 2-Isocyanatoethyl methacrylate

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:30674-80-7 SDS

30674-80-7Synthetic route

C22H25NO4

C22H25NO4

2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

Conditions
ConditionsYield
With isocyanurate at 200 - 250℃; for 200h;88%
C13H15NO4

C13H15NO4

2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

Conditions
ConditionsYield
With DURANATE TPA-100 In 1,2-dichloro-benzene at 250℃; under 6000.6 Torr; for 200h; Inert atmosphere;86%
(2-isocyanatoethyl) 3-chloro-2-methylpropionate

(2-isocyanatoethyl) 3-chloro-2-methylpropionate

2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

Conditions
ConditionsYield
With triethylamine In toluene at 75℃; for 30h; Product distribution / selectivity;70%
With quinoline at 160℃; for 1h; Product distribution / selectivity;
2-(N,N-diethylureido)ethyl methacrylate

2-(N,N-diethylureido)ethyl methacrylate

2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

Conditions
ConditionsYield
With hydrogenchloride; 2,6-di-tert-butyl-4-methyl-phenol In 5,5-dimethyl-1,3-cyclohexadiene at 130℃;66.7%
phosgene
75-44-5

phosgene

methacrylic acid-<2-amino-ethyl ester>-hydrochloride

methacrylic acid-<2-amino-ethyl ester>-hydrochloride

2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

Conditions
ConditionsYield
With toluene
phosgene
75-44-5

phosgene

2-isopropylidene-2-oxazoline
502422-79-9

2-isopropylidene-2-oxazoline

2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

2-aminoethylmethacrylate hydrochloride

2-aminoethylmethacrylate hydrochloride

2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: tetrahydrofuran / 4 h / 17 - 23 °C
2.1: toluene-4-sulfonic acid / toluene / 3.5 h / 23 - 30 °C
2.2: 8 h / 80 °C
View Scheme
Multi-step reaction with 2 steps
1: tetrahydrofuran / 4 h / 17 - 23 °C
2: toluene-4-sulfonic acid / toluene / 11.75 h / 23 - 80 °C
View Scheme
2-(1H-imidazole-1-carboxamido)ethyl methacrylate
89743-58-8

2-(1H-imidazole-1-carboxamido)ethyl methacrylate

2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

Conditions
ConditionsYield
Stage #1: 2-(1H-imidazole-1-carboxamido)ethyl methacrylate With toluene-4-sulfonic acid In toluene at 23 - 30℃; for 3.5h;
Stage #2: In toluene at 80℃; for 8h; Product distribution / selectivity;
With toluene-4-sulfonic acid In toluene at 23 - 80℃; for 11.75h; Product distribution / selectivity;
2-(2-methyl-acryloyloxy)-ethyl-ammonium tosylate
344920-47-4

2-(2-methyl-acryloyloxy)-ethyl-ammonium tosylate

2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: 10H-phenothiazine / ethyl acetate / 24.5 h / 30 °C
2.1: toluene-4-sulfonic acid / toluene / 3.5 h / 23 - 30 °C
2.2: 8 h / 80 °C
View Scheme
Multi-step reaction with 2 steps
1: 10H-phenothiazine / ethyl acetate / 24.5 h / 21 - 30 °C
2: toluene-4-sulfonic acid / toluene / 11.75 h / 23 - 80 °C
View Scheme
phosgene
75-44-5

phosgene

2-aminoethylmethacrylate hydrochloride

2-aminoethylmethacrylate hydrochloride

2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

Conditions
ConditionsYield
In toluene at 85℃;110 g
dimethyl 2-hydroxyethylphosphonate
54731-72-5

dimethyl 2-hydroxyethylphosphonate

2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

2-methyl-acrylic acid 2-[2-(dimethoxy-phosphoryl)-ethoxycarbonylamino]-ethyl ester
852610-27-6

2-methyl-acrylic acid 2-[2-(dimethoxy-phosphoryl)-ethoxycarbonylamino]-ethyl ester

Conditions
ConditionsYield
at 20℃; for 6h;100%
2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

hydroxymethyl-phosphonic acid dimethyl ester
24630-67-9

hydroxymethyl-phosphonic acid dimethyl ester

2-methyl-acrylic acid 2-(dimethoxy-phosphorylmethoxycarbonylamino)-ethyl ester
852610-26-5

2-methyl-acrylic acid 2-(dimethoxy-phosphorylmethoxycarbonylamino)-ethyl ester

Conditions
ConditionsYield
In toluene at 20℃; for 10h;100%
2,2-bis(hydroxymethyl)propionic acid
4767-03-7

2,2-bis(hydroxymethyl)propionic acid

2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

C19H28N2O10
304698-73-5

C19H28N2O10

Conditions
ConditionsYield
Stage #1: 2,2-bis(hydroxymethyl)propionic acid; 2-Isocyanatoethyl methacrylate With dibutyltin dilaurate In tetrahydrofuran at 20℃;
Stage #2: With methanol In tetrahydrofuran for 2h;
100%
4,6-O-benzylidene-2-amino-2-deoxy-methyl-α-D-glucopyranoside
128657-58-9

4,6-O-benzylidene-2-amino-2-deoxy-methyl-α-D-glucopyranoside

2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

C21H28N2O8
1242280-90-5

C21H28N2O8

Conditions
ConditionsYield
In tetrahydrofuran at 20℃;100%
2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

N-butylamine
109-73-9

N-butylamine

2-(4-butylureido)ethyl methacrylate
111653-59-9

2-(4-butylureido)ethyl methacrylate

Conditions
ConditionsYield
In dichloromethane100%
In dichloromethane at 0 - 20℃; Inert atmosphere;80%
2,2',2''-triaminotriethylamine
4097-89-6

2,2',2''-triaminotriethylamine

2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

2-methyl-18-methyl-8-[2-[[[[2-[(2-methyl-1-oxo-2-propen-1-yl)oxy]ethyl]amino]carbonyl]amino]ethyl]-4,12,17-trioxo-16-oxa-3,5,8,11,13-pentaazanonadec-18-en-1-yl-2-propenoic acid

2-methyl-18-methyl-8-[2-[[[[2-[(2-methyl-1-oxo-2-propen-1-yl)oxy]ethyl]amino]carbonyl]amino]ethyl]-4,12,17-trioxo-16-oxa-3,5,8,11,13-pentaazanonadec-18-en-1-yl-2-propenoic acid

Conditions
ConditionsYield
In dichloromethane at 0 - 20℃; for 4h;100%
phenyl(2,4,6-trimethylbenzoyl)phosphinic acid

phenyl(2,4,6-trimethylbenzoyl)phosphinic acid

2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

3-glycidoxypropyltrimethoxysilane
2530-83-8

3-glycidoxypropyltrimethoxysilane

C32H46NO11PSi

C32H46NO11PSi

Conditions
ConditionsYield
With triethylamine In n-heptane at 20℃; Inert atmosphere;100%
2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

N-phenyl-N-(3-trimethoxysilylpropyl)amine
3068-76-6

N-phenyl-N-(3-trimethoxysilylpropyl)amine

3,3-dimethoxy-8-oxo-7-phenyl-2-oxa-7,9-diaza-3-silaundecan-11-yl methacrylate

3,3-dimethoxy-8-oxo-7-phenyl-2-oxa-7,9-diaza-3-silaundecan-11-yl methacrylate

Conditions
ConditionsYield
at 50℃;100%
2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

(N-phenylaminomethyl) trimethoxysilane
77855-73-3

(N-phenylaminomethyl) trimethoxysilane

3,3-dimethoxy-6-oxo-5-phenyl-2-oxa-5,7-diaza-3-silanonan-9-yl methacrylate

3,3-dimethoxy-6-oxo-5-phenyl-2-oxa-5,7-diaza-3-silanonan-9-yl methacrylate

Conditions
ConditionsYield
at 50℃;100%
(3-(N-ethylamino)isobutyl) trimethoxysilane

(3-(N-ethylamino)isobutyl) trimethoxysilane

2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

7-ethyl-3,3-dimethoxy-5-methyl-8-oxo-2-oxa-7,9-diaza-3-silaundecan-11-yl methacrylate

7-ethyl-3,3-dimethoxy-5-methyl-8-oxo-2-oxa-7,9-diaza-3-silaundecan-11-yl methacrylate

Conditions
ConditionsYield
at 55℃;100%
2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

<(N-Butylamino)propyl>trimethoxysilane
31024-56-3

<(N-Butylamino)propyl>trimethoxysilane

7-butyl-3,3-dimethoxy-8-oxo-2-oxa-7,9-diaza-3-silaundecan-11-yl methacrylate
1560012-76-1

7-butyl-3,3-dimethoxy-8-oxo-2-oxa-7,9-diaza-3-silaundecan-11-yl methacrylate

Conditions
ConditionsYield
at 55℃;100%
2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

(4-aminobutyl)-triethoxysilane
3069-30-5

(4-aminobutyl)-triethoxysilane

4,4-diethoxy-10-oxo-3-oxa-9,11-diaza-4-silatridecan-13-yl methacrylate

4,4-diethoxy-10-oxo-3-oxa-9,11-diaza-4-silatridecan-13-yl methacrylate

Conditions
ConditionsYield
at 55℃;100%
(4-amino-3,3-dimethylbutyl)trimethoxysilane
157923-74-5

(4-amino-3,3-dimethylbutyl)trimethoxysilane

2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

3,3-dimethoxy-6,6-dimethyl-9-oxo-2-oxa-8,10-diaza-3-siladodecan-12-yl methacrylate

3,3-dimethoxy-6,6-dimethyl-9-oxo-2-oxa-8,10-diaza-3-siladodecan-12-yl methacrylate

Conditions
ConditionsYield
at 60℃;100%
2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

N-methyl-3-trimethoxysilylpropylamine
3069-25-8

N-methyl-3-trimethoxysilylpropylamine

3,3-dimethoxy-7-methyl-8-oxo-2-oxa-7,9-diaza-3-silaundecan-11-yl methacrylate
1560012-77-2

3,3-dimethoxy-7-methyl-8-oxo-2-oxa-7,9-diaza-3-silaundecan-11-yl methacrylate

Conditions
ConditionsYield
at 60℃;100%
2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

[1-(2-aminoethyl)-3-aminopropyl]trimethoxysilane
1760-24-3

[1-(2-aminoethyl)-3-aminopropyl]trimethoxysilane

4,9-dioxo-5-(3-(trimethoxysilyl)propyl)-3,5,8,10-tetraazadodecane-1,12-diyl bis(2-methylacrylate)

4,9-dioxo-5-(3-(trimethoxysilyl)propyl)-3,5,8,10-tetraazadodecane-1,12-diyl bis(2-methylacrylate)

Conditions
ConditionsYield
at 55℃;100%
2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

N-(6-aminohexyl)-3-aminopropyltrimethoxysilane

N-(6-aminohexyl)-3-aminopropyltrimethoxysilane

4,13-dioxo-5 -(3 -(trimethoxy silyl)propyl)-3 ,5,12,14-tetraazahexadecane-1,16-diyl bis(2-methyl acrylate)

4,13-dioxo-5 -(3 -(trimethoxy silyl)propyl)-3 ,5,12,14-tetraazahexadecane-1,16-diyl bis(2-methyl acrylate)

Conditions
ConditionsYield
at 55℃;100%
2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

N-(2-aminoethyl)-11aminoundecyl trimethoxysilane

N-(2-aminoethyl)-11aminoundecyl trimethoxysilane

4,9-dioxo-5-(11-(trimethoxysilyl)undecyl)-3,5,8,l0-tetraazadodecane-1,12-diyl bis(2-methylacrylate)

4,9-dioxo-5-(11-(trimethoxysilyl)undecyl)-3,5,8,l0-tetraazadodecane-1,12-diyl bis(2-methylacrylate)

Conditions
ConditionsYield
at 70℃;100%
2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

(N-cyclohexylaminopropyl) trimethoxysilane
3068-78-8

(N-cyclohexylaminopropyl) trimethoxysilane

7-cyclohexyl-3,3-dimethoxy-8-oxo-2-oxa-7,9-diaza-3-silaundecan-11-yl methacrylate

7-cyclohexyl-3,3-dimethoxy-8-oxo-2-oxa-7,9-diaza-3-silaundecan-11-yl methacrylate

Conditions
ConditionsYield
at 92℃; for 1h;100%
unilin 350
162730-22-5

unilin 350

2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

C50H92N2O8

C50H92N2O8

Conditions
ConditionsYield
With dibutyltin dilaurate at 85℃; for 3h; Inert atmosphere;100%
2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

1,1,1,3',3',3'-hexafluoro-propanol
920-66-1

1,1,1,3',3',3'-hexafluoro-propanol

C10H11F6NO4

C10H11F6NO4

Conditions
ConditionsYield
With 10H-phenothiazine; 4-methoxy-phenol at 50℃; for 24h; Temperature; Reagent/catalyst; Inert atmosphere; Green chemistry;99.6%
Tetraethylene glycol
112-60-7

Tetraethylene glycol

2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

16-hydroxy-4-oxo-5,8,11,14-tetraoxa-3-azahexadecyl methacrylate

16-hydroxy-4-oxo-5,8,11,14-tetraoxa-3-azahexadecyl methacrylate

Conditions
ConditionsYield
With dibutyltin dilaurate; 4-methoxy-phenol In diethyl ether at 40℃; for 12h; Solvent; Flow reactor;99.5%
With dibutyltin dilaurate; 4-methoxy-phenol In tetrahydrofuran at 75℃; for 5h;
2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

2,2'-[1,2-ethanediylbis(oxy)]bisethanol
112-27-6

2,2'-[1,2-ethanediylbis(oxy)]bisethanol

13-hydroxy-4-oxo-5,8,11-trioxa-3-azatridecyl methacrylate

13-hydroxy-4-oxo-5,8,11-trioxa-3-azatridecyl methacrylate

Conditions
ConditionsYield
With dibutyltin dilaurate; 4-methoxy-phenol In diethyl ether at 40℃; for 12h; Flow reactor;99.5%
With dibutyltin dilaurate; 4-methoxy-phenol In tetrahydrofuran at 75℃; for 5h;
2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

2-(2-(2-(2-hydroxypropoxy)propoxy)propoxy)propan-1-ol
24800-25-7

2-(2-(2-(2-hydroxypropoxy)propoxy)propoxy)propan-1-ol

16-hydroxy-6,9,12,15-tetramethyl- 4-oxo-5,8,11,14-tetraoxa-3-azahexadecyl methacrylate

16-hydroxy-6,9,12,15-tetramethyl- 4-oxo-5,8,11,14-tetraoxa-3-azahexadecyl methacrylate

Conditions
ConditionsYield
With dibutyltin dilaurate; 4-methoxy-phenol In diethyl ether at 40℃; for 12h; Flow reactor;99.4%
With dibutyltin dilaurate; 4-methoxy-phenol In tetrahydrofuran at 75℃; for 5h;
2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

6-methylisocytosine
3977-29-5

6-methylisocytosine

2-methylacrylic acid 2-[3-(6-methyloxo-1,4-dihydropyrinidin-2-yl)ureido]ethyl ester
474434-71-4

2-methylacrylic acid 2-[3-(6-methyloxo-1,4-dihydropyrinidin-2-yl)ureido]ethyl ester

Conditions
ConditionsYield
In dimethyl sulfoxide at 20℃; for 2h;99%
In dimethyl sulfoxide92%
In dimethyl sulfoxide90%
In dimethyl sulfoxide at 170℃;60%
In dimethyl sulfoxide at 150℃;
2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

3-amino-3-deoxy-α-D-allopyranosyl β-D-fructofuranoside
121784-13-2

3-amino-3-deoxy-α-D-allopyranosyl β-D-fructofuranoside

3-deoxy-3-N'-methacryloyloxyethylureido-α-D-allopyranosyl β-D-fructofuranoside
879291-40-4

3-deoxy-3-N'-methacryloyloxyethylureido-α-D-allopyranosyl β-D-fructofuranoside

Conditions
ConditionsYield
In water at 0 - 7℃;99%
2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

4-hydroxy-1-((1'-phenylethyl)oxy)-2,2,6,6-tetramethylpiperidine
132416-36-5

4-hydroxy-1-((1'-phenylethyl)oxy)-2,2,6,6-tetramethylpiperidine

4-(2'-methacryloyloxyethylcarbamyl)-1-((1'-phenylethyl)oxy)-2,2,6,6-tetramethylpiperidine
945656-07-5

4-(2'-methacryloyloxyethylcarbamyl)-1-((1'-phenylethyl)oxy)-2,2,6,6-tetramethylpiperidine

Conditions
ConditionsYield
With dibutyltin(II) dilaurate In N,N-dimethyl-formamide at 20℃; for 2h;99%
2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

6,7-dihydro-2-methyl-5H-pyrimido<1,2-d><1,2,4>thiadiazole-3(2H)-thione
112723-26-9

6,7-dihydro-2-methyl-5H-pyrimido<1,2-d><1,2,4>thiadiazole-3(2H)-thione

2-Methyl-acrylic acid 2-{3-[2-(2-methyl-acryloyloxy)-ethyl]-1,4-dioxo-3,4,6,7-tetrahydro-5H-2aλ4-thia-2,3,4a,7a-tetraaza-cyclopenta[cd]inden-2-yl}-ethyl ester
121058-60-4

2-Methyl-acrylic acid 2-{3-[2-(2-methyl-acryloyloxy)-ethyl]-1,4-dioxo-3,4,6,7-tetrahydro-5H-2aλ4-thia-2,3,4a,7a-tetraaza-cyclopenta[cd]inden-2-yl}-ethyl ester

Conditions
ConditionsYield
In chloroform for 24h; Heating;98%
2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

2,2’-((sulfonylbis(4,1-phenylene))bis(sulfanediyl))bis(ethan-1-ol)
53680-66-3

2,2’-((sulfonylbis(4,1-phenylene))bis(sulfanediyl))bis(ethan-1-ol)

4,4'-bis(methacryloyloxyethylcarbamatoethylthio)phenylsulfone
1048373-41-6

4,4'-bis(methacryloyloxyethylcarbamatoethylthio)phenylsulfone

Conditions
ConditionsYield
With triethylamine In acetonitrile at 20℃;98%
2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

N-hexadecyl-N-(2-hydroxyethyl)-N,N-dimethylammonium bromide
20317-32-2

N-hexadecyl-N-(2-hydroxyethyl)-N,N-dimethylammonium bromide

2-(methacryloyloxyethylcarbamoyloxy)ethyl hexadecylammonium bromide

2-(methacryloyloxyethylcarbamoyloxy)ethyl hexadecylammonium bromide

Conditions
ConditionsYield
With dibutyltin dilaurate In tetrahydrofuran at 40℃; for 24h;98%
6-amino-1-hexanol
4048-33-3

6-amino-1-hexanol

2-Isocyanatoethyl methacrylate
30674-80-7

2-Isocyanatoethyl methacrylate

2-[(6-hydroxyhexylamino)carbonylamino]ethylmethacrylate

2-[(6-hydroxyhexylamino)carbonylamino]ethylmethacrylate

Conditions
ConditionsYield
In dichloromethane at 0 - 20℃; for 2.25h;98%

30674-80-7Relevant articles and documents

COMPOSITION, PRODUCTION METHOD FOR COMPOSITION, AND PRODUCTION METHOD FOR UNSATURATED COMPOUND

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Paragraph 0131; 0132, (2021/07/02)

The invention relates to a composition excellent in stability during storage and stability during utilization, and relates to a method of producing the composition. The composition includes a compound (A) represented by general formula (1) and a compound (B) represented by general formula (2), and includes 0.00002 to 0.2 parts by mass of the compound (B) with respect to 100 parts by mass of the compound (A), [in-line-formulae](R1—COO)n—R2—(NCO)m??(1)[/in-line-formulae] [in-line-formulae](R1—COO)n—R2—(R3—R1)m??(2)[/in-line-formulae] wherein in general formulae (1) and (2), R1 is an ethylenically unsaturated group having 2 to 7 carbon atoms; R2 is a (m+n)-valent hydrocarbon group having 1 to 7 carbon atoms and optionally contains an ether group; R1 and R2 in the general formula (1) are the same as R1 and R2 in the general formula (2); in general formula (2), R3 is —NHC(═O)—; and n and m each represent an integer of one or two.

ISOCYANATE PRODUCTION METHOD

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Paragraph 0447-0450; 0459; 0478, (2020/05/02)

An isocyanate production method according to the present invention is a method in which an isocyanate is produced by subjecting a carbamate to thermal decomposition, and includes: a step of preparing a mixture liquid containing the carbamate, an inactive solvent and a polyisocyanate compound; a step of conducting a thermal decomposition reaction of the carbamate by continuously introducing the mixture liquid into a thermal decomposition reactor; a step of collecting a low-boiling decomposition product by continuously extracting the low-boiling decomposition product in a gaseous state from the reactor, the low-boiling decomposition product having a boiling point lower than the polyisocyanate compound; and a step of collecting a high-boiling component by continuously extracting, from the reactor, a liquid phase component which is not collected in a gaseous state at the step of collecting the low-boiling decomposition product.

COMPOSITION, CURABLE COMPOSITION, PRODUCTION METHOD THEREFOR, AND CURED PRODUCT

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Paragraph 0162-0163, (2017/01/12)

A composition is provided which includes a polymerizable compound (A) which includes a (meth)acryloyl group and an isocyanate group in a molecule thereof; and a reaction accelerator (B) which is a compound including a (meth)acryloyl group and a halogenated carbamoyl group in a molecule.

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