(4-(ethoxycarbonyl)phenyl)zinc chloride

Base Information

Chemical Name:(4-(ethoxycarbonyl)phenyl)zinc chloride
CAS No.:261516-38-5
Molecular Formula:C₉H₉ClO₂Zn
Molecular Weight:250.012
Hs Code.:

Synonyms:(4-(ethoxycarbonyl)phenyl)zinc chloride

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Chemical Property of (4-(ethoxycarbonyl)phenyl)zinc chloride

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Technology Process of (4-(ethoxycarbonyl)phenyl)zinc chloride

There total 2 articles about (4-(ethoxycarbonyl)phenyl)zinc chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 51934-41-9
4-iodobenzoic acid ethyl ester

: 7646-85-7,24359-56-6
zinc(II) chloride

: 261516-38-5
(4-(ethoxycarbonyl)phenyl)zinc chloride

Guidance literature:: 4-iodobenzoic acid ethyl ester; With TurboGrignard; In tetrahydrofuran; at -30 ℃; for 0.5h; Schlenk technique; Inert atmosphere;

zinc(II) chloride; In tetrahydrofuran; at 0 - 25 ℃; for 0.25h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.8b03787

Reference yield: 6.0%

: 7335-27-5
ethyl 4-chlorobenzoate

: 7440-66-6
zinc

: 261516-38-5
(4-(ethoxycarbonyl)phenyl)zinc chloride

: 93-89-0,99341-95-4
benzoic acid ethyl ester

: 47230-38-6
diethyl biphenyl-4,4'-dicarboxylate

Guidance literature:: With trifluoroacetic acid; cobalt(II) bromide; zinc dibromide; In acetonitrile; the mixt. in CH3CN was stirred at room temp., then arylbromide was added, stirred at room temp.; GC analysis;
DOI:10.1021/ja0289494