1,3,5-tris(N-acetyl-N-(2,3-dihydroxy-5-sulfobenzyl)aminomethyl)benzene trisodium salt

Base Information

Chemical Name:1,3,5-tris(N-acetyl-N-(2,3-dihydroxy-5-sulfobenzyl)aminomethyl)benzene trisodium salt
CAS No.:79087-39-1
Molecular Formula:C₃₆H₃₆N₃O₁₈S₃*3Na
Molecular Weight:963.858
Hs Code.:

Synonyms:1,3,5-tris(N-acetyl-N-(2,3-dihydroxy-5-sulfobenzyl)aminomethyl)benzene trisodium salt

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Chemical Property of 1,3,5-tris(N-acetyl-N-(2,3-dihydroxy-5-sulfobenzyl)aminomethyl)benzene trisodium salt

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Technology Process of 1,3,5-tris(N-acetyl-N-(2,3-dihydroxy-5-sulfobenzyl)aminomethyl)benzene trisodium salt

There total 3 articles about 1,3,5-tris(N-acetyl-N-(2,3-dihydroxy-5-sulfobenzyl)aminomethyl)benzene trisodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 79105-36-5
1,3,5-tris(N-acetyl-N-(2,3-dihydroxybenzyl)aminomethyl)benzene

: 79087-39-1
1,3,5-tris(N-acetyl-N-(2,3-dihydroxy-5-sulfobenzyl)aminomethyl)benzene trisodium salt

Guidance literature:: With sulfuric acid; sulfur trioxide; Ambient temperature;
DOI:10.1021/ja00407a030

Reference yield:

: 79087-38-0
1,3,5-tris(N-acetyl-N-(2,3-dimethoxybenzyl)aminomethyl)benzene

: 79087-39-1
1,3,5-tris(N-acetyl-N-(2,3-dihydroxy-5-sulfobenzyl)aminomethyl)benzene trisodium salt

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / BBr₃ / CH₂Cl₂ / 20 - 25 °C

2: 80 percent / SO₃/H₂SO₄ / Ambient temperature

With sulfuric acid; sulfur trioxide; boron tribromide; In dichloromethane;
DOI:10.1021/ja00407a030

Reference yield:

: 79087-37-9
1,3,5-tris(N-(2,3-dimethoxybenzyl)aminomethyl)benzene trihydrochloride

: 79087-39-1
1,3,5-tris(N-acetyl-N-(2,3-dihydroxy-5-sulfobenzyl)aminomethyl)benzene trisodium salt

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / triethylamine / tetrahydrofuran / 20 - 25 °C

2: 65 percent / BBr₃ / CH₂Cl₂ / 20 - 25 °C

3: 80 percent / SO₃/H₂SO₄ / Ambient temperature

With sulfuric acid; sulfur trioxide; boron tribromide; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00407a030