1,3,5-tris(N-acetyl-N-(2,3-dimethoxybenzyl)aminomethyl)benzene

Base Information

• Chemical Name: 1,3,5-tris(N-acetyl-N-(2,3-dimethoxybenzyl)aminomethyl)benzene
• CAS No.: 79087-38-0
• Molecular Formula: C₄₂H₅₁N₃O₉
• Molecular Weight: 741.882
• Mol file: 79087-38-0.mol

Synonyms:1,3,5-tris(N-acetyl-N-(2,3-dimethoxybenzyl)aminomethyl)benzene

Chemical Property of 1,3,5-tris(N-acetyl-N-(2,3-dimethoxybenzyl)aminomethyl)benzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3,5-tris(N-acetyl-N-(2,3-dimethoxybenzyl)aminomethyl)benzene

There total 1 articles about 1,3,5-tris(N-acetyl-N-(2,3-dimethoxybenzyl)aminomethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

1,3,5-tris(N-(2,3-dimethoxybenzyl)aminomethyl)benzene trihydrochloride (79087-37-9) + acetyl chloride (75-36-5) → 1,3,5-tris(N-acetyl-N-(2,3-dimethoxybenzyl)aminomethyl)benzene (79087-38-0)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 - 25 ℃;

DOI:10.1021/ja00407a030

Reference yield:

1,3,5-tris(N-acetyl-N-(2,3-dimethoxybenzyl)aminomethyl)benzene (79087-38-0) → 1,3,5-tris(N-acetyl-N-(2,3-dihydroxy-5-sulfobenzyl)aminomethyl)benzene trisodium salt (79087-39-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / BBr₃ / CH₂Cl₂ / 20 - 25 °C

2: 80 percent / SO₃/H₂SO₄ / Ambient temperature

With sulfuric acid; sulfur trioxide; boron tribromide; In dichloromethane;

DOI:10.1021/ja00407a030

upstream raw materials:

1,3,5-tris(N-(2,3-dimethoxybenzyl)aminomethyl)benzene trihydrochloride

acetyl chloride

Downstream raw materials:

1,3,5-tris(N-acetyl-N-(2,3-dihydroxy-5-sulfobenzyl)aminomethyl)benzene trisodium salt