1,3,5-tris(N-(2,3-dimethoxybenzyl)aminomethyl)benzene trihydrochloride

Base Information

Chemical Name:1,3,5-tris(N-(2,3-dimethoxybenzyl)aminomethyl)benzene trihydrochloride
CAS No.:79087-37-9
Molecular Formula:C₃₆H₄₅N₃O₆*3ClH
Molecular Weight:725.153
Hs Code.:

Synonyms:1,3,5-tris(N-(2,3-dimethoxybenzyl)aminomethyl)benzene trihydrochloride

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Chemical Property of 1,3,5-tris(N-(2,3-dimethoxybenzyl)aminomethyl)benzene trihydrochloride

Chemical Property:

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Technology Process of 1,3,5-tris(N-(2,3-dimethoxybenzyl)aminomethyl)benzene trihydrochloride

There total 1 articles about 1,3,5-tris(N-(2,3-dimethoxybenzyl)aminomethyl)benzene trihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 71353-08-7
Benzene-1,3,5-tricarboxylic acid tris-(2,3-dimethoxy-benzylamide)

: 79087-37-9
1,3,5-tris(N-(2,3-dimethoxybenzyl)aminomethyl)benzene trihydrochloride

Guidance literature:: With borane; In tetrahydrofuran; for 60h; Heating;
DOI:10.1021/ja00407a030

Reference yield: 45.0%

: 79087-37-9
1,3,5-tris(N-(2,3-dimethoxybenzyl)aminomethyl)benzene trihydrochloride

: 75-36-5
acetyl chloride

: 79087-38-0
1,3,5-tris(N-acetyl-N-(2,3-dimethoxybenzyl)aminomethyl)benzene

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 - 25 ℃;
DOI:10.1021/ja00407a030

Reference yield:

: 79087-37-9
1,3,5-tris(N-(2,3-dimethoxybenzyl)aminomethyl)benzene trihydrochloride

: 79087-39-1
1,3,5-tris(N-acetyl-N-(2,3-dihydroxy-5-sulfobenzyl)aminomethyl)benzene trisodium salt

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / triethylamine / tetrahydrofuran / 20 - 25 °C

2: 65 percent / BBr₃ / CH₂Cl₂ / 20 - 25 °C

3: 80 percent / SO₃/H₂SO₄ / Ambient temperature

With sulfuric acid; sulfur trioxide; boron tribromide; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00407a030