4-Acetyl-N-benzyl-N-<(benzyloxy)carbonyl>-5-oxohexylamine

Base Information

Chemical Name:4-Acetyl-N-benzyl-N-<(benzyloxy)carbonyl>-5-oxohexylamine
CAS No.:86953-68-6
Molecular Formula:C₂₃H₂₇NO₄
Molecular Weight:381.472
Hs Code.:

Synonyms:4-Acetyl-N-benzyl-N-<(benzyloxy)carbonyl>-5-oxohexylamine

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Chemical Property of 4-Acetyl-N-benzyl-N-<(benzyloxy)carbonyl>-5-oxohexylamine

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Technology Process of 4-Acetyl-N-benzyl-N-<(benzyloxy)carbonyl>-5-oxohexylamine

There total 4 articles about 4-Acetyl-N-benzyl-N-<(benzyloxy)carbonyl>-5-oxohexylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.4%

: 86953-67-5
N-Benzyl-N<(benzyloxy)carbonyl>-3-bromopropylamine

: 123-54-6,81235-32-7
acetylacetone

: 86953-68-6
4-Acetyl-N-benzyl-N-<(benzyloxy)carbonyl>-5-oxohexylamine

Guidance literature:: With 18-crown-6 ether; potassium carbonate; potassium iodide; In butanone; for 15h; Heating;
DOI:10.1021/jo00170a037

Reference yield:

: 86954-09-8
N-benzyl-3-((tetrahydro-2H-pyran-2-yl)oxy)propane-1-amine

: 86953-68-6
4-Acetyl-N-benzyl-N-<(benzyloxy)carbonyl>-5-oxohexylamine

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃ / acetone

2: 96.4 percent / p-toluenesulfonic acid / methanol / 5 h / Ambient temperature

3: 92.5 percent / CBr₄, PPh₃ / acetonitrile / Ambient temperature

4: 64.4 percent / K₂CO₃, KI, 18-crown-6 / butan-2-one / 15 h / Heating

With 18-crown-6 ether; carbon tetrabromide; potassium carbonate; toluene-4-sulfonic acid; triphenylphosphine; potassium iodide; In methanol; acetone; acetonitrile; butanone;
DOI:10.1021/jo00170a037

Reference yield:

: 86953-66-4
3-amino>-1-propanol

: 86953-68-6
4-Acetyl-N-benzyl-N-<(benzyloxy)carbonyl>-5-oxohexylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 92.5 percent / CBr₄, PPh₃ / acetonitrile / Ambient temperature

2: 64.4 percent / K₂CO₃, KI, 18-crown-6 / butan-2-one / 15 h / Heating

With 18-crown-6 ether; carbon tetrabromide; potassium carbonate; triphenylphosphine; potassium iodide; In acetonitrile; butanone;
DOI:10.1021/jo00170a037