ethyl 1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hepto-1,4-furanuronate

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Chemical Name:ethyl 1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hepto-1,4-furanuronate
CAS No.:86632-11-3
Molecular Formula:C₃₅H₃₁N₅O₈
Molecular Weight:649.66
Hs Code.:

Synonyms:ethyl 1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hepto-1,4-furanuronate

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Chemical Property of ethyl 1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hepto-1,4-furanuronate

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Technology Process of ethyl 1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hepto-1,4-furanuronate

There total 3 articles about ethyl 1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hepto-1,4-furanuronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 86632-10-2
ethyl 1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hept-5-eno-1,4-furanuronate

: 86632-11-3
ethyl 1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hepto-1,4-furanuronate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; acetic acid; for 32h; under 3102.9 Torr;
DOI:10.1021/jm00364a033

Reference yield:

: 57018-84-5
N⁶-benzoyl-9-(β-D-arabino-2,3-di-O-benzoyl-1,5-pentodialdofuranosyl)adenine

: 86632-11-3
ethyl 1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hepto-1,4-furanuronate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 3 h

2: 85 percent / H₂ / 10percent Pd/C / ethanol; acetic acid / 32 h / 3102.9 Torr

With pyridine; hydrogen; palladium on activated charcoal; In ethanol; acetic acid;
DOI:10.1021/jm00364a033

Reference yield:

: 57018-83-4
O²,O³-dibenzoyl-1-(6-benzoylamino-purin-9-yl)-β-D-1-deoxy-arabinofuranose

: 86632-11-3
ethyl 1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hepto-1,4-furanuronate

Guidance literature:: Multi-step reaction with 3 steps

1: DMSO, N,N'-dicyclohexylcarbodiimide (DCC), dichloroacetic acid

2: pyridine / 3 h

3: 85 percent / H₂ / 10percent Pd/C / ethanol; acetic acid / 32 h / 3102.9 Torr

With pyridine; dichloro-acetic acid; hydrogen; dimethyl sulfoxide; dicyclohexyl-carbodiimide; palladium on activated charcoal; In ethanol; acetic acid;
DOI:10.1021/jm00364a033